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Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection

via simple hydrothermal method, CeO(2) was in-situ grown onto the CNTs to form CeO(2)/CNTs nanocomposites were synthesized with cerium nitrate as Ce resource. The morphology and structure were characterized by transmission electron microscopy and X-ray diffraction. The characterizations reveal that...

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Detalles Bibliográficos
Autores principales: Hu, Chao, Huang, Haiping, Yan, Yu, Hu, Yongmei, Liu, Sui-Jun, Wen, He-Rui
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Frontiers Media S.A. 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9152013/
https://www.ncbi.nlm.nih.gov/pubmed/35655701
http://dx.doi.org/10.3389/fchem.2022.907777
Descripción
Sumario:via simple hydrothermal method, CeO(2) was in-situ grown onto the CNTs to form CeO(2)/CNTs nanocomposites were synthesized with cerium nitrate as Ce resource. The morphology and structure were characterized by transmission electron microscopy and X-ray diffraction. The characterizations reveal that CeO(2) nanoparticles are uniformly dispersed onto the surface of the pre-acidified CNTs. The electrochemical property of the synthesized nanocomposite was investigated in 0.1 M KCl electrolyte containing 2 mM [Fe(CN)(6)](3-/4-). The nanocomposites were employed to fabricate electrochemical sensor for phenol detection. The linear range for phenol detection measured by the differential pulse voltammetry method is 1–500 μM. The sensor also exhibits good selectivity, reproducibility and stability. When applied for the river and tap water analysis, it shows good recovery rate.