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Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection

via simple hydrothermal method, CeO(2) was in-situ grown onto the CNTs to form CeO(2)/CNTs nanocomposites were synthesized with cerium nitrate as Ce resource. The morphology and structure were characterized by transmission electron microscopy and X-ray diffraction. The characterizations reveal that...

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Autores principales: Hu, Chao, Huang, Haiping, Yan, Yu, Hu, Yongmei, Liu, Sui-Jun, Wen, He-Rui
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Frontiers Media S.A. 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9152013/
https://www.ncbi.nlm.nih.gov/pubmed/35655701
http://dx.doi.org/10.3389/fchem.2022.907777
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author Hu, Chao
Huang, Haiping
Yan, Yu
Hu, Yongmei
Liu, Sui-Jun
Wen, He-Rui
author_facet Hu, Chao
Huang, Haiping
Yan, Yu
Hu, Yongmei
Liu, Sui-Jun
Wen, He-Rui
author_sort Hu, Chao
collection PubMed
description via simple hydrothermal method, CeO(2) was in-situ grown onto the CNTs to form CeO(2)/CNTs nanocomposites were synthesized with cerium nitrate as Ce resource. The morphology and structure were characterized by transmission electron microscopy and X-ray diffraction. The characterizations reveal that CeO(2) nanoparticles are uniformly dispersed onto the surface of the pre-acidified CNTs. The electrochemical property of the synthesized nanocomposite was investigated in 0.1 M KCl electrolyte containing 2 mM [Fe(CN)(6)](3-/4-). The nanocomposites were employed to fabricate electrochemical sensor for phenol detection. The linear range for phenol detection measured by the differential pulse voltammetry method is 1–500 μM. The sensor also exhibits good selectivity, reproducibility and stability. When applied for the river and tap water analysis, it shows good recovery rate.
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spelling pubmed-91520132022-06-01 Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection Hu, Chao Huang, Haiping Yan, Yu Hu, Yongmei Liu, Sui-Jun Wen, He-Rui Front Chem Chemistry via simple hydrothermal method, CeO(2) was in-situ grown onto the CNTs to form CeO(2)/CNTs nanocomposites were synthesized with cerium nitrate as Ce resource. The morphology and structure were characterized by transmission electron microscopy and X-ray diffraction. The characterizations reveal that CeO(2) nanoparticles are uniformly dispersed onto the surface of the pre-acidified CNTs. The electrochemical property of the synthesized nanocomposite was investigated in 0.1 M KCl electrolyte containing 2 mM [Fe(CN)(6)](3-/4-). The nanocomposites were employed to fabricate electrochemical sensor for phenol detection. The linear range for phenol detection measured by the differential pulse voltammetry method is 1–500 μM. The sensor also exhibits good selectivity, reproducibility and stability. When applied for the river and tap water analysis, it shows good recovery rate. Frontiers Media S.A. 2022-05-17 /pmc/articles/PMC9152013/ /pubmed/35655701 http://dx.doi.org/10.3389/fchem.2022.907777 Text en Copyright © 2022 Hu, Huang, Yan, Hu, Liu and Wen. https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms.
spellingShingle Chemistry
Hu, Chao
Huang, Haiping
Yan, Yu
Hu, Yongmei
Liu, Sui-Jun
Wen, He-Rui
Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection
title Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection
title_full Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection
title_fullStr Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection
title_full_unstemmed Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection
title_short Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection
title_sort simple synthesis of ceo(2) nanoparticle composites in situ grown on carbon nanotubes for phenol detection
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9152013/
https://www.ncbi.nlm.nih.gov/pubmed/35655701
http://dx.doi.org/10.3389/fchem.2022.907777
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