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The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel

To further improve the mechanical properties of H13 steel at room and high temperatures, its precipitates were regulated based on the Thermo-Calc results. Scanning electron microscope (SEM), electron backscattering diffraction (EBSD), transmission electron microscope (TEM), and X-ray diffraction (XR...

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Autores principales: Shi, Kefei, Zhao, Fei, Liu, Yuan, Yin, Sheng, Yang, Ronggui
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9181995/
https://www.ncbi.nlm.nih.gov/pubmed/35683271
http://dx.doi.org/10.3390/ma15113970
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author Shi, Kefei
Zhao, Fei
Liu, Yuan
Yin, Sheng
Yang, Ronggui
author_facet Shi, Kefei
Zhao, Fei
Liu, Yuan
Yin, Sheng
Yang, Ronggui
author_sort Shi, Kefei
collection PubMed
description To further improve the mechanical properties of H13 steel at room and high temperatures, its precipitates were regulated based on the Thermo-Calc results. Scanning electron microscope (SEM), electron backscattering diffraction (EBSD), transmission electron microscope (TEM), and X-ray diffraction (XRD) Rietveld refinement were used to study the effect of the intercritical annealing on the microstructure and mechanical properties of H13 steel. The results show that the intercritical annealing at 850~95 °C increased the VC volume fraction from 2.23 to 3.03~3.48%. Increasing the VC volume fraction could inhibit the M(7)C(3) precipitation from 10.01 to 6.63~5.72% during tempering. A large amount of VC also promoted the M(23)C(6) precipitation during tempering at higher dislocation densities. The intercortical annealing simultaneously increased the elongation of H13 steel. An excellent combination (room temperature: ultimate tensile strength (UTS) of 898 MPa and total elongation (TEL) of 19.35%, 650 °C: UTS of 439 MPa, and TEL of 27.80%) could be obtained when intercritical annealing is performed at 900 °C. Meanwhile, after aging at 650 °C for 128 h, the room temperature UTS and TEL decreased by only 31 MPa and 0.52%, respectively.
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spelling pubmed-91819952022-06-10 The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel Shi, Kefei Zhao, Fei Liu, Yuan Yin, Sheng Yang, Ronggui Materials (Basel) Article To further improve the mechanical properties of H13 steel at room and high temperatures, its precipitates were regulated based on the Thermo-Calc results. Scanning electron microscope (SEM), electron backscattering diffraction (EBSD), transmission electron microscope (TEM), and X-ray diffraction (XRD) Rietveld refinement were used to study the effect of the intercritical annealing on the microstructure and mechanical properties of H13 steel. The results show that the intercritical annealing at 850~95 °C increased the VC volume fraction from 2.23 to 3.03~3.48%. Increasing the VC volume fraction could inhibit the M(7)C(3) precipitation from 10.01 to 6.63~5.72% during tempering. A large amount of VC also promoted the M(23)C(6) precipitation during tempering at higher dislocation densities. The intercortical annealing simultaneously increased the elongation of H13 steel. An excellent combination (room temperature: ultimate tensile strength (UTS) of 898 MPa and total elongation (TEL) of 19.35%, 650 °C: UTS of 439 MPa, and TEL of 27.80%) could be obtained when intercritical annealing is performed at 900 °C. Meanwhile, after aging at 650 °C for 128 h, the room temperature UTS and TEL decreased by only 31 MPa and 0.52%, respectively. MDPI 2022-06-02 /pmc/articles/PMC9181995/ /pubmed/35683271 http://dx.doi.org/10.3390/ma15113970 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Shi, Kefei
Zhao, Fei
Liu, Yuan
Yin, Sheng
Yang, Ronggui
The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel
title The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel
title_full The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel
title_fullStr The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel
title_full_unstemmed The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel
title_short The Effect of the Pre-Existing VC on the Evolution of Precipitate and Mechanical Properties in the H13 Steel
title_sort effect of the pre-existing vc on the evolution of precipitate and mechanical properties in the h13 steel
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9181995/
https://www.ncbi.nlm.nih.gov/pubmed/35683271
http://dx.doi.org/10.3390/ma15113970
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