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Facile Synthesis of Mesoporous Silica at Room Temperature for CO(2) Adsorption

Although mesoporous silica materials have been widely investigated for many applications, most silica materials are made by calcination processes. We successfully developed a convenient method to synthesize mesoporous materials at room temperature. Although the silica materials made by the two diffe...

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Detalles Bibliográficos
Autores principales: Kang, Misun, Lee, Jong-tak, Kim, Min-Kyoung, Byun, Myunghwan, Bae, Jae-Young
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9227262/
https://www.ncbi.nlm.nih.gov/pubmed/35744541
http://dx.doi.org/10.3390/mi13060926
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author Kang, Misun
Lee, Jong-tak
Kim, Min-Kyoung
Byun, Myunghwan
Bae, Jae-Young
author_facet Kang, Misun
Lee, Jong-tak
Kim, Min-Kyoung
Byun, Myunghwan
Bae, Jae-Young
author_sort Kang, Misun
collection PubMed
description Although mesoporous silica materials have been widely investigated for many applications, most silica materials are made by calcination processes. We successfully developed a convenient method to synthesize mesoporous materials at room temperature. Although the silica materials made by the two different methods, which are the calcination process and the room-temperature process, have similar specific surface areas, the silica materials produced with the room-temperature process have a significantly larger pore volume. This larger pore volume has the potential to attach to functional groups that can be applied to various industrial fields such as CO(2) adsorption. This mesoporous silica with a larger pore volume was analyzed by TEM, FT-IR, low angle X-ray diffraction, N(2)-adsorption analysis, and CO(2) adsorption experiments in comparison with the mesoporous silica synthesized with the traditional calcination method.
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spelling pubmed-92272622022-06-25 Facile Synthesis of Mesoporous Silica at Room Temperature for CO(2) Adsorption Kang, Misun Lee, Jong-tak Kim, Min-Kyoung Byun, Myunghwan Bae, Jae-Young Micromachines (Basel) Article Although mesoporous silica materials have been widely investigated for many applications, most silica materials are made by calcination processes. We successfully developed a convenient method to synthesize mesoporous materials at room temperature. Although the silica materials made by the two different methods, which are the calcination process and the room-temperature process, have similar specific surface areas, the silica materials produced with the room-temperature process have a significantly larger pore volume. This larger pore volume has the potential to attach to functional groups that can be applied to various industrial fields such as CO(2) adsorption. This mesoporous silica with a larger pore volume was analyzed by TEM, FT-IR, low angle X-ray diffraction, N(2)-adsorption analysis, and CO(2) adsorption experiments in comparison with the mesoporous silica synthesized with the traditional calcination method. MDPI 2022-06-10 /pmc/articles/PMC9227262/ /pubmed/35744541 http://dx.doi.org/10.3390/mi13060926 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kang, Misun
Lee, Jong-tak
Kim, Min-Kyoung
Byun, Myunghwan
Bae, Jae-Young
Facile Synthesis of Mesoporous Silica at Room Temperature for CO(2) Adsorption
title Facile Synthesis of Mesoporous Silica at Room Temperature for CO(2) Adsorption
title_full Facile Synthesis of Mesoporous Silica at Room Temperature for CO(2) Adsorption
title_fullStr Facile Synthesis of Mesoporous Silica at Room Temperature for CO(2) Adsorption
title_full_unstemmed Facile Synthesis of Mesoporous Silica at Room Temperature for CO(2) Adsorption
title_short Facile Synthesis of Mesoporous Silica at Room Temperature for CO(2) Adsorption
title_sort facile synthesis of mesoporous silica at room temperature for co(2) adsorption
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9227262/
https://www.ncbi.nlm.nih.gov/pubmed/35744541
http://dx.doi.org/10.3390/mi13060926
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