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Microstructure and Phase Evolution of Ti-Al-C-Nb Composites Prepared by In Situ Selective Laser Forming

In the present work, a novel Ti-Al-C-Nb composite was prepared using in situ selective laser forming (ISLF). The formation mechanism of the Ti-Al-C-Nb bulks, which were synthesized using elemental titanium, aluminum, and carbon (graphite) powders via ISLF techniques, was investigated. The results sh...

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Autores principales: Zhang, Kai, Li, Shurui, Yan, Zhilong, Xiong, Zhiwei, Bakoutas, Desti Dorion Likoundayenda, Liu, Tingting, Liao, Wenhe
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9230832/
https://www.ncbi.nlm.nih.gov/pubmed/35744409
http://dx.doi.org/10.3390/ma15124351
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author Zhang, Kai
Li, Shurui
Yan, Zhilong
Xiong, Zhiwei
Bakoutas, Desti Dorion Likoundayenda
Liu, Tingting
Liao, Wenhe
author_facet Zhang, Kai
Li, Shurui
Yan, Zhilong
Xiong, Zhiwei
Bakoutas, Desti Dorion Likoundayenda
Liu, Tingting
Liao, Wenhe
author_sort Zhang, Kai
collection PubMed
description In the present work, a novel Ti-Al-C-Nb composite was prepared using in situ selective laser forming (ISLF). The formation mechanism of the Ti-Al-C-Nb bulks, which were synthesized using elemental titanium, aluminum, and carbon (graphite) powders via ISLF techniques, was investigated. The results showed that the Ti(3)Al and TiC phases were the dominant synthesis products during the chemical reactions, and these occurred during the ISLF process. The size of the fine nanoscale crystal TiC grains could reach 157 nm at an energy level of 60 J/mm(3). The porous structure of the ISLF specimens was disclosed, and an open porosity of 20–44% was determined via the scanning speed and the laser power. Both the high dynamic viscosity and the reactions of the raw powders led to the generation of a considerable number of pores, whereas the specimen processed using 45 W and 100 mm/s possessed the lowest degree of open porosity.
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spelling pubmed-92308322022-06-25 Microstructure and Phase Evolution of Ti-Al-C-Nb Composites Prepared by In Situ Selective Laser Forming Zhang, Kai Li, Shurui Yan, Zhilong Xiong, Zhiwei Bakoutas, Desti Dorion Likoundayenda Liu, Tingting Liao, Wenhe Materials (Basel) Article In the present work, a novel Ti-Al-C-Nb composite was prepared using in situ selective laser forming (ISLF). The formation mechanism of the Ti-Al-C-Nb bulks, which were synthesized using elemental titanium, aluminum, and carbon (graphite) powders via ISLF techniques, was investigated. The results showed that the Ti(3)Al and TiC phases were the dominant synthesis products during the chemical reactions, and these occurred during the ISLF process. The size of the fine nanoscale crystal TiC grains could reach 157 nm at an energy level of 60 J/mm(3). The porous structure of the ISLF specimens was disclosed, and an open porosity of 20–44% was determined via the scanning speed and the laser power. Both the high dynamic viscosity and the reactions of the raw powders led to the generation of a considerable number of pores, whereas the specimen processed using 45 W and 100 mm/s possessed the lowest degree of open porosity. MDPI 2022-06-20 /pmc/articles/PMC9230832/ /pubmed/35744409 http://dx.doi.org/10.3390/ma15124351 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Zhang, Kai
Li, Shurui
Yan, Zhilong
Xiong, Zhiwei
Bakoutas, Desti Dorion Likoundayenda
Liu, Tingting
Liao, Wenhe
Microstructure and Phase Evolution of Ti-Al-C-Nb Composites Prepared by In Situ Selective Laser Forming
title Microstructure and Phase Evolution of Ti-Al-C-Nb Composites Prepared by In Situ Selective Laser Forming
title_full Microstructure and Phase Evolution of Ti-Al-C-Nb Composites Prepared by In Situ Selective Laser Forming
title_fullStr Microstructure and Phase Evolution of Ti-Al-C-Nb Composites Prepared by In Situ Selective Laser Forming
title_full_unstemmed Microstructure and Phase Evolution of Ti-Al-C-Nb Composites Prepared by In Situ Selective Laser Forming
title_short Microstructure and Phase Evolution of Ti-Al-C-Nb Composites Prepared by In Situ Selective Laser Forming
title_sort microstructure and phase evolution of ti-al-c-nb composites prepared by in situ selective laser forming
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9230832/
https://www.ncbi.nlm.nih.gov/pubmed/35744409
http://dx.doi.org/10.3390/ma15124351
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