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Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons

Mg–15Gd–1Zn (wt.%) alloy was successfully prepared via the spark plasma sintering rapid solidification ribbons process. Microstructure investigation showed that the sintered alloys consisted of fine grains, the β(1) phase, and long-perioded stacking ordered phase (LPSO). The sintering temperature an...

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Detalles Bibliográficos
Autores principales: Luo, Wenbo, Guo, Yanke, Xue, Zhiyong, Han, Xiuzhu, Kong, Qinke, Mu, Minghao, Zhang, Gaolong, Mao, Weimin, Ren, Yu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9243015/
https://www.ncbi.nlm.nih.gov/pubmed/35768495
http://dx.doi.org/10.1038/s41598-022-14753-2
Descripción
Sumario:Mg–15Gd–1Zn (wt.%) alloy was successfully prepared via the spark plasma sintering rapid solidification ribbons process. Microstructure investigation showed that the sintered alloys consisted of fine grains, the β(1) phase, and long-perioded stacking ordered phase (LPSO). The sintering temperature and time have a significant effect on the microstructural evolution. A lower sintering temperature (430 °C ) was beneficial for obtaining finer grain sizes with less than 5 μm and a higher content of β(1) phase with a content of 3–15 vol.% and a size-distribution of (10–600) nm. A higher temperature for a longer sintering time, 450–470 °C and 5–10 min, helpfully promoted precipitating the abundantly lamellar LPSO phase, and its content was 2–10 vol.% for LPSO phase with the width of (10–100) nm. The mechanical properties indicated that the fine grain size and supersaturated solid solution contributed at least 50% of the yield stress, and the residual contribution was related to the β(1) phase and LPSO phase strengthening, which were based on their contents and the sizes.