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Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons

Mg–15Gd–1Zn (wt.%) alloy was successfully prepared via the spark plasma sintering rapid solidification ribbons process. Microstructure investigation showed that the sintered alloys consisted of fine grains, the β(1) phase, and long-perioded stacking ordered phase (LPSO). The sintering temperature an...

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Autores principales: Luo, Wenbo, Guo, Yanke, Xue, Zhiyong, Han, Xiuzhu, Kong, Qinke, Mu, Minghao, Zhang, Gaolong, Mao, Weimin, Ren, Yu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9243015/
https://www.ncbi.nlm.nih.gov/pubmed/35768495
http://dx.doi.org/10.1038/s41598-022-14753-2
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author Luo, Wenbo
Guo, Yanke
Xue, Zhiyong
Han, Xiuzhu
Kong, Qinke
Mu, Minghao
Zhang, Gaolong
Mao, Weimin
Ren, Yu
author_facet Luo, Wenbo
Guo, Yanke
Xue, Zhiyong
Han, Xiuzhu
Kong, Qinke
Mu, Minghao
Zhang, Gaolong
Mao, Weimin
Ren, Yu
author_sort Luo, Wenbo
collection PubMed
description Mg–15Gd–1Zn (wt.%) alloy was successfully prepared via the spark plasma sintering rapid solidification ribbons process. Microstructure investigation showed that the sintered alloys consisted of fine grains, the β(1) phase, and long-perioded stacking ordered phase (LPSO). The sintering temperature and time have a significant effect on the microstructural evolution. A lower sintering temperature (430 °C ) was beneficial for obtaining finer grain sizes with less than 5 μm and a higher content of β(1) phase with a content of 3–15 vol.% and a size-distribution of (10–600) nm. A higher temperature for a longer sintering time, 450–470 °C and 5–10 min, helpfully promoted precipitating the abundantly lamellar LPSO phase, and its content was 2–10 vol.% for LPSO phase with the width of (10–100) nm. The mechanical properties indicated that the fine grain size and supersaturated solid solution contributed at least 50% of the yield stress, and the residual contribution was related to the β(1) phase and LPSO phase strengthening, which were based on their contents and the sizes.
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spelling pubmed-92430152022-07-01 Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons Luo, Wenbo Guo, Yanke Xue, Zhiyong Han, Xiuzhu Kong, Qinke Mu, Minghao Zhang, Gaolong Mao, Weimin Ren, Yu Sci Rep Article Mg–15Gd–1Zn (wt.%) alloy was successfully prepared via the spark plasma sintering rapid solidification ribbons process. Microstructure investigation showed that the sintered alloys consisted of fine grains, the β(1) phase, and long-perioded stacking ordered phase (LPSO). The sintering temperature and time have a significant effect on the microstructural evolution. A lower sintering temperature (430 °C ) was beneficial for obtaining finer grain sizes with less than 5 μm and a higher content of β(1) phase with a content of 3–15 vol.% and a size-distribution of (10–600) nm. A higher temperature for a longer sintering time, 450–470 °C and 5–10 min, helpfully promoted precipitating the abundantly lamellar LPSO phase, and its content was 2–10 vol.% for LPSO phase with the width of (10–100) nm. The mechanical properties indicated that the fine grain size and supersaturated solid solution contributed at least 50% of the yield stress, and the residual contribution was related to the β(1) phase and LPSO phase strengthening, which were based on their contents and the sizes. Nature Publishing Group UK 2022-06-29 /pmc/articles/PMC9243015/ /pubmed/35768495 http://dx.doi.org/10.1038/s41598-022-14753-2 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Luo, Wenbo
Guo, Yanke
Xue, Zhiyong
Han, Xiuzhu
Kong, Qinke
Mu, Minghao
Zhang, Gaolong
Mao, Weimin
Ren, Yu
Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons
title Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons
title_full Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons
title_fullStr Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons
title_full_unstemmed Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons
title_short Microstructure and mechanical properties of the Mg–Gd–Zn alloy prepared by sintering of rapidly-solidified ribbons
title_sort microstructure and mechanical properties of the mg–gd–zn alloy prepared by sintering of rapidly-solidified ribbons
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9243015/
https://www.ncbi.nlm.nih.gov/pubmed/35768495
http://dx.doi.org/10.1038/s41598-022-14753-2
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