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Polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine

Magnetic solid phase extraction (MSPE) have been widely applied in a variety of sample preparation techniques. Herein, Fe(3)O(4)@pDA as the sorbents for MSPE, were developed for the determination of phenolic acids and flavonoids in fruit wine samples in combination with LC-MS/MS. The Fe(3)O(4)@pDA w...

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Autores principales: Lee, Hui-Ling, Kang, Chih-Yuan, Kuo, Yen-Jung, Tseng, Shan-Ni
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Taiwan Food and Drug Administration 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9261790/
https://www.ncbi.nlm.nih.gov/pubmed/35696245
http://dx.doi.org/10.38212/2224-6614.3359
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author Lee, Hui-Ling
Kang, Chih-Yuan
Kuo, Yen-Jung
Tseng, Shan-Ni
author_facet Lee, Hui-Ling
Kang, Chih-Yuan
Kuo, Yen-Jung
Tseng, Shan-Ni
author_sort Lee, Hui-Ling
collection PubMed
description Magnetic solid phase extraction (MSPE) have been widely applied in a variety of sample preparation techniques. Herein, Fe(3)O(4)@pDA as the sorbents for MSPE, were developed for the determination of phenolic acids and flavonoids in fruit wine samples in combination with LC-MS/MS. The Fe(3)O(4)@pDA were characterized by Fourier transform infrared spectroscopy (FT-IR), powder X-ray diffraction (PXRD), transmission electron microscopy (TEM), Superconducting Quantum Interference Device Magnetometer (SQUID) and thermogravimetric analysis (TGA) in detail. In the present study, a new, rapid, and efficient MSPE by LC-MS/MS was established for the extraction and sensitive detection of phenolic acids and flavonoids. Under the optimized condition of extraction procedure including the pH value of 4.0, 10 mg of Fe(3)O(4)@pDA, 60 s extraction time, and 600 μL desorption solvent volume, good responses were investigated. Results showed that the limits of detection (S/N = 3) for phenolic acids and flavonoids were in the range of 0.01–0.29 ng/ mL. The correlation coefficients of all analytes were more than 0.9985. The method was satisfactorily used for the detection of eleven analytes, and the recoveries of these targets for the two spiked wines (white grape wine and litchi wine) ranged from 80.03 to 116.68% and from 84.00 to 116.1%, respectively.
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spelling pubmed-92617902022-07-18 Polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine Lee, Hui-Ling Kang, Chih-Yuan Kuo, Yen-Jung Tseng, Shan-Ni J Food Drug Anal Original Article Magnetic solid phase extraction (MSPE) have been widely applied in a variety of sample preparation techniques. Herein, Fe(3)O(4)@pDA as the sorbents for MSPE, were developed for the determination of phenolic acids and flavonoids in fruit wine samples in combination with LC-MS/MS. The Fe(3)O(4)@pDA were characterized by Fourier transform infrared spectroscopy (FT-IR), powder X-ray diffraction (PXRD), transmission electron microscopy (TEM), Superconducting Quantum Interference Device Magnetometer (SQUID) and thermogravimetric analysis (TGA) in detail. In the present study, a new, rapid, and efficient MSPE by LC-MS/MS was established for the extraction and sensitive detection of phenolic acids and flavonoids. Under the optimized condition of extraction procedure including the pH value of 4.0, 10 mg of Fe(3)O(4)@pDA, 60 s extraction time, and 600 μL desorption solvent volume, good responses were investigated. Results showed that the limits of detection (S/N = 3) for phenolic acids and flavonoids were in the range of 0.01–0.29 ng/ mL. The correlation coefficients of all analytes were more than 0.9985. The method was satisfactorily used for the detection of eleven analytes, and the recoveries of these targets for the two spiked wines (white grape wine and litchi wine) ranged from 80.03 to 116.68% and from 84.00 to 116.1%, respectively. Taiwan Food and Drug Administration 2021-09-15 /pmc/articles/PMC9261790/ /pubmed/35696245 http://dx.doi.org/10.38212/2224-6614.3359 Text en © 2021 Taiwan Food and Drug Administration https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC-BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/ (https://creativecommons.org/licenses/by-nc-nd/4.0/) ).
spellingShingle Original Article
Lee, Hui-Ling
Kang, Chih-Yuan
Kuo, Yen-Jung
Tseng, Shan-Ni
Polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine
title Polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine
title_full Polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine
title_fullStr Polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine
title_full_unstemmed Polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine
title_short Polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine
title_sort polydopamine and silica nanoparticles magnetic solid phase extraction coupled with liquid chromatography-tandem mass spectrometry to determine phenolic acids and flavonoids in fruit wine
topic Original Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9261790/
https://www.ncbi.nlm.nih.gov/pubmed/35696245
http://dx.doi.org/10.38212/2224-6614.3359
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