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A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material

Porous iron-based scaffolds were prepared by the simple replica method using polyurethane foam as a template and applying the sintering process in a tube furnace. Their surface morphology was characterized using scanning electron microscopy (SEM) and phase homogeneity was confirmed using X-ray diffr...

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Autores principales: Grodzicka, Marlena, Gąsior, Gabriela, Wiśniewski, Marek, Bartmański, Michał, Radtke, Aleksandra
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9267498/
https://www.ncbi.nlm.nih.gov/pubmed/35806677
http://dx.doi.org/10.3390/ma15134552
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author Grodzicka, Marlena
Gąsior, Gabriela
Wiśniewski, Marek
Bartmański, Michał
Radtke, Aleksandra
author_facet Grodzicka, Marlena
Gąsior, Gabriela
Wiśniewski, Marek
Bartmański, Michał
Radtke, Aleksandra
author_sort Grodzicka, Marlena
collection PubMed
description Porous iron-based scaffolds were prepared by the simple replica method using polyurethane foam as a template and applying the sintering process in a tube furnace. Their surface morphology was characterized using scanning electron microscopy (SEM) and phase homogeneity was confirmed using X-ray diffraction (XRD). Corrosion behavior was determined using immersion and potentiodynamic polarization methods in phosphate buffered saline (PBS). The surface energy was calculated by studying the changes of enthalpy of calorimetric immersion. A preliminary biological test was also carried out and was done using the albumin adsorption procedure. Results of our work showed that in using the simple replica method it is possible to obtain iron biomaterial with morphology and mechanical properties almost identical to bones, and possessing adequate wettability, which gives the potential to use this material as biomaterial for scaffolds in orthopedics.
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spelling pubmed-92674982022-07-09 A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material Grodzicka, Marlena Gąsior, Gabriela Wiśniewski, Marek Bartmański, Michał Radtke, Aleksandra Materials (Basel) Article Porous iron-based scaffolds were prepared by the simple replica method using polyurethane foam as a template and applying the sintering process in a tube furnace. Their surface morphology was characterized using scanning electron microscopy (SEM) and phase homogeneity was confirmed using X-ray diffraction (XRD). Corrosion behavior was determined using immersion and potentiodynamic polarization methods in phosphate buffered saline (PBS). The surface energy was calculated by studying the changes of enthalpy of calorimetric immersion. A preliminary biological test was also carried out and was done using the albumin adsorption procedure. Results of our work showed that in using the simple replica method it is possible to obtain iron biomaterial with morphology and mechanical properties almost identical to bones, and possessing adequate wettability, which gives the potential to use this material as biomaterial for scaffolds in orthopedics. MDPI 2022-06-28 /pmc/articles/PMC9267498/ /pubmed/35806677 http://dx.doi.org/10.3390/ma15134552 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Grodzicka, Marlena
Gąsior, Gabriela
Wiśniewski, Marek
Bartmański, Michał
Radtke, Aleksandra
A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material
title A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material
title_full A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material
title_fullStr A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material
title_full_unstemmed A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material
title_short A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material
title_sort simple replica method as the way to obtain a morphologically and mechanically bone-like iron-based biodegradable material
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9267498/
https://www.ncbi.nlm.nih.gov/pubmed/35806677
http://dx.doi.org/10.3390/ma15134552
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