Cargando…

Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks

Light scattering and turbidimetry techniques are classical tools for characterizing the dynamics and structure of single nanoparticles or nanostructured networks. They work by analyzing, as a function of time (Dynamic Light Scattering, DLS) or angles (Static Light Scattering, SLS), the light scatter...

Descripción completa

Detalles Bibliográficos
Autores principales: Anzini, Pietro, Redoglio, Daniele, Rocco, Mattia, Masciocchi, Norberto, Ferri, Fabio
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9268389/
https://www.ncbi.nlm.nih.gov/pubmed/35808049
http://dx.doi.org/10.3390/nano12132214
_version_ 1784743969611055104
author Anzini, Pietro
Redoglio, Daniele
Rocco, Mattia
Masciocchi, Norberto
Ferri, Fabio
author_facet Anzini, Pietro
Redoglio, Daniele
Rocco, Mattia
Masciocchi, Norberto
Ferri, Fabio
author_sort Anzini, Pietro
collection PubMed
description Light scattering and turbidimetry techniques are classical tools for characterizing the dynamics and structure of single nanoparticles or nanostructured networks. They work by analyzing, as a function of time (Dynamic Light Scattering, DLS) or angles (Static Light Scattering, SLS), the light scattered by a sample, or measuring, as a function of the wavelength, the intensity scattered over the entire solid angle when the sample is illuminated with white light (Multi Wavelength Turbidimetry, MWT). Light scattering methods probe different length scales, in the ranges of [Formula: see text] (DLS), or [Formula: see text] (Wide Angle SLS), or [Formula: see text] (Low Angle SLS), and some of them can be operated in a time-resolved mode, with the possibility of characterizing not only stationary, but also aggregating, polymerizing, or self-assembling samples. Thus, the combined use of these techniques represents a powerful approach for studying systems characterized by very different length scales. In this work, we will review some typical applications of these methods, ranging from the field of colloidal fractal aggregation to the polymerization of biologic networks made of randomly entangled nanosized fibers. We will also discuss the opportunity of combining together different scattering techniques, emphasizing the advantages of a global analysis with respect to single-methods data processing.
format Online
Article
Text
id pubmed-9268389
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-92683892022-07-09 Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks Anzini, Pietro Redoglio, Daniele Rocco, Mattia Masciocchi, Norberto Ferri, Fabio Nanomaterials (Basel) Review Light scattering and turbidimetry techniques are classical tools for characterizing the dynamics and structure of single nanoparticles or nanostructured networks. They work by analyzing, as a function of time (Dynamic Light Scattering, DLS) or angles (Static Light Scattering, SLS), the light scattered by a sample, or measuring, as a function of the wavelength, the intensity scattered over the entire solid angle when the sample is illuminated with white light (Multi Wavelength Turbidimetry, MWT). Light scattering methods probe different length scales, in the ranges of [Formula: see text] (DLS), or [Formula: see text] (Wide Angle SLS), or [Formula: see text] (Low Angle SLS), and some of them can be operated in a time-resolved mode, with the possibility of characterizing not only stationary, but also aggregating, polymerizing, or self-assembling samples. Thus, the combined use of these techniques represents a powerful approach for studying systems characterized by very different length scales. In this work, we will review some typical applications of these methods, ranging from the field of colloidal fractal aggregation to the polymerization of biologic networks made of randomly entangled nanosized fibers. We will also discuss the opportunity of combining together different scattering techniques, emphasizing the advantages of a global analysis with respect to single-methods data processing. MDPI 2022-06-28 /pmc/articles/PMC9268389/ /pubmed/35808049 http://dx.doi.org/10.3390/nano12132214 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Review
Anzini, Pietro
Redoglio, Daniele
Rocco, Mattia
Masciocchi, Norberto
Ferri, Fabio
Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks
title Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks
title_full Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks
title_fullStr Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks
title_full_unstemmed Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks
title_short Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks
title_sort light scattering and turbidimetry techniques for the characterization of nanoparticles and nanostructured networks
topic Review
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9268389/
https://www.ncbi.nlm.nih.gov/pubmed/35808049
http://dx.doi.org/10.3390/nano12132214
work_keys_str_mv AT anzinipietro lightscatteringandturbidimetrytechniquesforthecharacterizationofnanoparticlesandnanostructurednetworks
AT redogliodaniele lightscatteringandturbidimetrytechniquesforthecharacterizationofnanoparticlesandnanostructurednetworks
AT roccomattia lightscatteringandturbidimetrytechniquesforthecharacterizationofnanoparticlesandnanostructurednetworks
AT masciocchinorberto lightscatteringandturbidimetrytechniquesforthecharacterizationofnanoparticlesandnanostructurednetworks
AT ferrifabio lightscatteringandturbidimetrytechniquesforthecharacterizationofnanoparticlesandnanostructurednetworks