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Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks
Light scattering and turbidimetry techniques are classical tools for characterizing the dynamics and structure of single nanoparticles or nanostructured networks. They work by analyzing, as a function of time (Dynamic Light Scattering, DLS) or angles (Static Light Scattering, SLS), the light scatter...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9268389/ https://www.ncbi.nlm.nih.gov/pubmed/35808049 http://dx.doi.org/10.3390/nano12132214 |
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author | Anzini, Pietro Redoglio, Daniele Rocco, Mattia Masciocchi, Norberto Ferri, Fabio |
author_facet | Anzini, Pietro Redoglio, Daniele Rocco, Mattia Masciocchi, Norberto Ferri, Fabio |
author_sort | Anzini, Pietro |
collection | PubMed |
description | Light scattering and turbidimetry techniques are classical tools for characterizing the dynamics and structure of single nanoparticles or nanostructured networks. They work by analyzing, as a function of time (Dynamic Light Scattering, DLS) or angles (Static Light Scattering, SLS), the light scattered by a sample, or measuring, as a function of the wavelength, the intensity scattered over the entire solid angle when the sample is illuminated with white light (Multi Wavelength Turbidimetry, MWT). Light scattering methods probe different length scales, in the ranges of [Formula: see text] (DLS), or [Formula: see text] (Wide Angle SLS), or [Formula: see text] (Low Angle SLS), and some of them can be operated in a time-resolved mode, with the possibility of characterizing not only stationary, but also aggregating, polymerizing, or self-assembling samples. Thus, the combined use of these techniques represents a powerful approach for studying systems characterized by very different length scales. In this work, we will review some typical applications of these methods, ranging from the field of colloidal fractal aggregation to the polymerization of biologic networks made of randomly entangled nanosized fibers. We will also discuss the opportunity of combining together different scattering techniques, emphasizing the advantages of a global analysis with respect to single-methods data processing. |
format | Online Article Text |
id | pubmed-9268389 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-92683892022-07-09 Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks Anzini, Pietro Redoglio, Daniele Rocco, Mattia Masciocchi, Norberto Ferri, Fabio Nanomaterials (Basel) Review Light scattering and turbidimetry techniques are classical tools for characterizing the dynamics and structure of single nanoparticles or nanostructured networks. They work by analyzing, as a function of time (Dynamic Light Scattering, DLS) or angles (Static Light Scattering, SLS), the light scattered by a sample, or measuring, as a function of the wavelength, the intensity scattered over the entire solid angle when the sample is illuminated with white light (Multi Wavelength Turbidimetry, MWT). Light scattering methods probe different length scales, in the ranges of [Formula: see text] (DLS), or [Formula: see text] (Wide Angle SLS), or [Formula: see text] (Low Angle SLS), and some of them can be operated in a time-resolved mode, with the possibility of characterizing not only stationary, but also aggregating, polymerizing, or self-assembling samples. Thus, the combined use of these techniques represents a powerful approach for studying systems characterized by very different length scales. In this work, we will review some typical applications of these methods, ranging from the field of colloidal fractal aggregation to the polymerization of biologic networks made of randomly entangled nanosized fibers. We will also discuss the opportunity of combining together different scattering techniques, emphasizing the advantages of a global analysis with respect to single-methods data processing. MDPI 2022-06-28 /pmc/articles/PMC9268389/ /pubmed/35808049 http://dx.doi.org/10.3390/nano12132214 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Review Anzini, Pietro Redoglio, Daniele Rocco, Mattia Masciocchi, Norberto Ferri, Fabio Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks |
title | Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks |
title_full | Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks |
title_fullStr | Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks |
title_full_unstemmed | Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks |
title_short | Light Scattering and Turbidimetry Techniques for the Characterization of Nanoparticles and Nanostructured Networks |
title_sort | light scattering and turbidimetry techniques for the characterization of nanoparticles and nanostructured networks |
topic | Review |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9268389/ https://www.ncbi.nlm.nih.gov/pubmed/35808049 http://dx.doi.org/10.3390/nano12132214 |
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