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3D-Printed Nanocomposite Denture-Base Resins: Effect of ZrO(2) Nanoparticles on the Mechanical and Surface Properties In Vitro
Due to the low mechanical performances of 3D-printed denture base resins, ZrO(2) nanoparticles (ZrO(2)NPs) were incorporated into different 3D-printed resins and their effects on the flexure strength, elastic modulus, impact strength, hardness, and surface roughness were evaluated. A total of 286 sp...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9315924/ https://www.ncbi.nlm.nih.gov/pubmed/35889675 http://dx.doi.org/10.3390/nano12142451 |
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author | Alshaikh, Ali A. Khattar, Abdulrahman Almindil, Ibrahim A. Alsaif, Majed H. Akhtar, Sultan Khan, Soban Q. Gad, Mohammed M. |
author_facet | Alshaikh, Ali A. Khattar, Abdulrahman Almindil, Ibrahim A. Alsaif, Majed H. Akhtar, Sultan Khan, Soban Q. Gad, Mohammed M. |
author_sort | Alshaikh, Ali A. |
collection | PubMed |
description | Due to the low mechanical performances of 3D-printed denture base resins, ZrO(2) nanoparticles (ZrO(2)NPs) were incorporated into different 3D-printed resins and their effects on the flexure strength, elastic modulus, impact strength, hardness, and surface roughness were evaluated. A total of 286 specimens were fabricated in dimensions per respective test and divided according to materials into three groups: heat-polymerized as a control group and two 3D-printed resins (NextDent and ASIGA) which were modified with 0.5 wt.%, 1 wt.%, 3 wt.%, and 5 wt.% ZrO(2)NPs. The flexure strength and elastic modulus, impact strength, hardness, and surface roughness (µm) were measured using the three-point bending test, Charpy’s impact test, Vickers hardness test, and a profilometer, respectively. The data were analyzed by ANOVA and Tukey’s post hoc test (α = 0.05). The results showed that, in comparison to heat-polymerized resin, the unmodified 3D-printed resins showed a significant decrease in all tested properties (p < 0.001) except surface roughness (p = 0.11). In between 3D-printed resins, the addition of ZrO(2)NPs to 3D-printed resins showed a significant increase in flexure strength, impact strength, and hardness (p < 0.05) while showing no significant differences in surface roughness and elastic modulus (p > 0.05). Our study demonstrated that the unmodified 3D-printed resins showed inferior mechanical behavior when compared with heat-polymerized acrylic resin while the addition of ZrO(2)NPs improved the properties of 3D-printed resins. Therefore, the introduced 3D-printable nanocomposite denture-base resins are suitable for clinical use. |
format | Online Article Text |
id | pubmed-9315924 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-93159242022-07-27 3D-Printed Nanocomposite Denture-Base Resins: Effect of ZrO(2) Nanoparticles on the Mechanical and Surface Properties In Vitro Alshaikh, Ali A. Khattar, Abdulrahman Almindil, Ibrahim A. Alsaif, Majed H. Akhtar, Sultan Khan, Soban Q. Gad, Mohammed M. Nanomaterials (Basel) Article Due to the low mechanical performances of 3D-printed denture base resins, ZrO(2) nanoparticles (ZrO(2)NPs) were incorporated into different 3D-printed resins and their effects on the flexure strength, elastic modulus, impact strength, hardness, and surface roughness were evaluated. A total of 286 specimens were fabricated in dimensions per respective test and divided according to materials into three groups: heat-polymerized as a control group and two 3D-printed resins (NextDent and ASIGA) which were modified with 0.5 wt.%, 1 wt.%, 3 wt.%, and 5 wt.% ZrO(2)NPs. The flexure strength and elastic modulus, impact strength, hardness, and surface roughness (µm) were measured using the three-point bending test, Charpy’s impact test, Vickers hardness test, and a profilometer, respectively. The data were analyzed by ANOVA and Tukey’s post hoc test (α = 0.05). The results showed that, in comparison to heat-polymerized resin, the unmodified 3D-printed resins showed a significant decrease in all tested properties (p < 0.001) except surface roughness (p = 0.11). In between 3D-printed resins, the addition of ZrO(2)NPs to 3D-printed resins showed a significant increase in flexure strength, impact strength, and hardness (p < 0.05) while showing no significant differences in surface roughness and elastic modulus (p > 0.05). Our study demonstrated that the unmodified 3D-printed resins showed inferior mechanical behavior when compared with heat-polymerized acrylic resin while the addition of ZrO(2)NPs improved the properties of 3D-printed resins. Therefore, the introduced 3D-printable nanocomposite denture-base resins are suitable for clinical use. MDPI 2022-07-18 /pmc/articles/PMC9315924/ /pubmed/35889675 http://dx.doi.org/10.3390/nano12142451 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Alshaikh, Ali A. Khattar, Abdulrahman Almindil, Ibrahim A. Alsaif, Majed H. Akhtar, Sultan Khan, Soban Q. Gad, Mohammed M. 3D-Printed Nanocomposite Denture-Base Resins: Effect of ZrO(2) Nanoparticles on the Mechanical and Surface Properties In Vitro |
title | 3D-Printed Nanocomposite Denture-Base Resins: Effect of ZrO(2) Nanoparticles on the Mechanical and Surface Properties In Vitro |
title_full | 3D-Printed Nanocomposite Denture-Base Resins: Effect of ZrO(2) Nanoparticles on the Mechanical and Surface Properties In Vitro |
title_fullStr | 3D-Printed Nanocomposite Denture-Base Resins: Effect of ZrO(2) Nanoparticles on the Mechanical and Surface Properties In Vitro |
title_full_unstemmed | 3D-Printed Nanocomposite Denture-Base Resins: Effect of ZrO(2) Nanoparticles on the Mechanical and Surface Properties In Vitro |
title_short | 3D-Printed Nanocomposite Denture-Base Resins: Effect of ZrO(2) Nanoparticles on the Mechanical and Surface Properties In Vitro |
title_sort | 3d-printed nanocomposite denture-base resins: effect of zro(2) nanoparticles on the mechanical and surface properties in vitro |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9315924/ https://www.ncbi.nlm.nih.gov/pubmed/35889675 http://dx.doi.org/10.3390/nano12142451 |
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