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The Relationship between Microstructure and Fracture Behavior of TiAl/Ti(2)AlNb SPDB Joint with High Temperature Titanium Alloy Interlayers

In this paper, spark plasma diffusion bonding technology was employed to join TiAl and Ti(2)AlNb with high temperature titanium alloy interlayer at 950 °C/10kN/60 min, then following furnace cooling at cooling rate up to 100 °C/min. After welding, the joint was aging heat-treated at 800 °C for 24 h....

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Detalles Bibliográficos
Autores principales: Liao, Minxing, Tian, Hao, Zhao, Lei, Zhang, Boxian, He, Jianchao
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9316006/
https://www.ncbi.nlm.nih.gov/pubmed/35888316
http://dx.doi.org/10.3390/ma15144849
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author Liao, Minxing
Tian, Hao
Zhao, Lei
Zhang, Boxian
He, Jianchao
author_facet Liao, Minxing
Tian, Hao
Zhao, Lei
Zhang, Boxian
He, Jianchao
author_sort Liao, Minxing
collection PubMed
description In this paper, spark plasma diffusion bonding technology was employed to join TiAl and Ti(2)AlNb with high temperature titanium alloy interlayer at 950 °C/10kN/60 min, then following furnace cooling at cooling rate up to 100 °C/min. After welding, the joint was aging heat-treated at 800 °C for 24 h. The microstructure and the elements diffusion of the TiAl/Ti(2)AlNb joint was analyzed by field emission scanning electron microscopy (FESEM) with EDS. Moreover, the tensile properties of the joint were tested at room temperature, 650 °C, and 750 °C. The results show that the spark plasma diffusion bonding formed a high quality TiAl/Ti(2)AlNb joint without microcracks or microvoids, while also effectively protecting the base metal. Significant differences in the microstructure of the joint appeared from TiAl side to Ti(2)AlNb side: TiAl BM (Base Metal) → DP(Duplex) and NG (Near-Gamma) → α(2)-phase matrix with needle-like α-phase → bulk α(2)-phase → needle-like α-phase → metastable β-phase → Ti(2)AlNb BM. After heat treatment at 800 °C for 24 h, the microstructure of the TiAl side and the interlayer region did not change, but the density and size of the needle-like α-phase in region 3 increased slightly. The microstructure of Ti(2)AlNb near the weld changed obviously, and a large number of fine O phases are precipitated from the metastable β phase matrix after heat treatment. Except for the Ti(2)AlN near-interface region, the effect of heat treatment on the microstructure of the joint is not significant. The microhardness of the joint is in the shape of a mountain peak. The maximum microhardness at the interface is above 500 HV, and it is significantly reduced to 400 HV after heat treatment. The fracture of the joint occurred at the interface at room temperature, 650 °C, and 750 °C. with the tensile strength 450 MPa, 540 MPa, and 471 Mpa, respectively, and mainly showing brittle fracture.
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spelling pubmed-93160062022-07-27 The Relationship between Microstructure and Fracture Behavior of TiAl/Ti(2)AlNb SPDB Joint with High Temperature Titanium Alloy Interlayers Liao, Minxing Tian, Hao Zhao, Lei Zhang, Boxian He, Jianchao Materials (Basel) Article In this paper, spark plasma diffusion bonding technology was employed to join TiAl and Ti(2)AlNb with high temperature titanium alloy interlayer at 950 °C/10kN/60 min, then following furnace cooling at cooling rate up to 100 °C/min. After welding, the joint was aging heat-treated at 800 °C for 24 h. The microstructure and the elements diffusion of the TiAl/Ti(2)AlNb joint was analyzed by field emission scanning electron microscopy (FESEM) with EDS. Moreover, the tensile properties of the joint were tested at room temperature, 650 °C, and 750 °C. The results show that the spark plasma diffusion bonding formed a high quality TiAl/Ti(2)AlNb joint without microcracks or microvoids, while also effectively protecting the base metal. Significant differences in the microstructure of the joint appeared from TiAl side to Ti(2)AlNb side: TiAl BM (Base Metal) → DP(Duplex) and NG (Near-Gamma) → α(2)-phase matrix with needle-like α-phase → bulk α(2)-phase → needle-like α-phase → metastable β-phase → Ti(2)AlNb BM. After heat treatment at 800 °C for 24 h, the microstructure of the TiAl side and the interlayer region did not change, but the density and size of the needle-like α-phase in region 3 increased slightly. The microstructure of Ti(2)AlNb near the weld changed obviously, and a large number of fine O phases are precipitated from the metastable β phase matrix after heat treatment. Except for the Ti(2)AlN near-interface region, the effect of heat treatment on the microstructure of the joint is not significant. The microhardness of the joint is in the shape of a mountain peak. The maximum microhardness at the interface is above 500 HV, and it is significantly reduced to 400 HV after heat treatment. The fracture of the joint occurred at the interface at room temperature, 650 °C, and 750 °C. with the tensile strength 450 MPa, 540 MPa, and 471 Mpa, respectively, and mainly showing brittle fracture. MDPI 2022-07-12 /pmc/articles/PMC9316006/ /pubmed/35888316 http://dx.doi.org/10.3390/ma15144849 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Liao, Minxing
Tian, Hao
Zhao, Lei
Zhang, Boxian
He, Jianchao
The Relationship between Microstructure and Fracture Behavior of TiAl/Ti(2)AlNb SPDB Joint with High Temperature Titanium Alloy Interlayers
title The Relationship between Microstructure and Fracture Behavior of TiAl/Ti(2)AlNb SPDB Joint with High Temperature Titanium Alloy Interlayers
title_full The Relationship between Microstructure and Fracture Behavior of TiAl/Ti(2)AlNb SPDB Joint with High Temperature Titanium Alloy Interlayers
title_fullStr The Relationship between Microstructure and Fracture Behavior of TiAl/Ti(2)AlNb SPDB Joint with High Temperature Titanium Alloy Interlayers
title_full_unstemmed The Relationship between Microstructure and Fracture Behavior of TiAl/Ti(2)AlNb SPDB Joint with High Temperature Titanium Alloy Interlayers
title_short The Relationship between Microstructure and Fracture Behavior of TiAl/Ti(2)AlNb SPDB Joint with High Temperature Titanium Alloy Interlayers
title_sort relationship between microstructure and fracture behavior of tial/ti(2)alnb spdb joint with high temperature titanium alloy interlayers
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9316006/
https://www.ncbi.nlm.nih.gov/pubmed/35888316
http://dx.doi.org/10.3390/ma15144849
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