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Microwave-assisted extraction of pectin from grape pomace

The utilization of microwave technique for the pectin extraction from grape pomace (Fetească Neagră and Rară Neagră), its influence on yield, galacturonic acid content, degree of esterification and molecular weight of pectin were analyzed. The optimal conditions of the extraction process were microw...

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Autores principales: Spinei, Mariana, Oroian, Mircea
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9325980/
https://www.ncbi.nlm.nih.gov/pubmed/35882905
http://dx.doi.org/10.1038/s41598-022-16858-0
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author Spinei, Mariana
Oroian, Mircea
author_facet Spinei, Mariana
Oroian, Mircea
author_sort Spinei, Mariana
collection PubMed
description The utilization of microwave technique for the pectin extraction from grape pomace (Fetească Neagră and Rară Neagră), its influence on yield, galacturonic acid content, degree of esterification and molecular weight of pectin were analyzed. The optimal conditions of the extraction process were microwave power of 560 W, pH of 1.8 for 120 s. The pectin samples extracted by MAE in optimal conditions were analyzed by comparing with commercial apple and citrus pectin based on FT-IR analysis, thermal behavior, rheological characteristics and microstructure. The FT-IR analysis established the presence of different functional groups which are attributed to the finger print region of extracted pectin, while the rheological behavior presented a good viscoelasticity of pectin solutions. The obtained data assumes that grape pomace has a great potential to be a valuable source of pectin which can be extracted by simple and quick techniques, while maintaining analogous quality to conventional sources of pectin.
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spelling pubmed-93259802022-07-28 Microwave-assisted extraction of pectin from grape pomace Spinei, Mariana Oroian, Mircea Sci Rep Article The utilization of microwave technique for the pectin extraction from grape pomace (Fetească Neagră and Rară Neagră), its influence on yield, galacturonic acid content, degree of esterification and molecular weight of pectin were analyzed. The optimal conditions of the extraction process were microwave power of 560 W, pH of 1.8 for 120 s. The pectin samples extracted by MAE in optimal conditions were analyzed by comparing with commercial apple and citrus pectin based on FT-IR analysis, thermal behavior, rheological characteristics and microstructure. The FT-IR analysis established the presence of different functional groups which are attributed to the finger print region of extracted pectin, while the rheological behavior presented a good viscoelasticity of pectin solutions. The obtained data assumes that grape pomace has a great potential to be a valuable source of pectin which can be extracted by simple and quick techniques, while maintaining analogous quality to conventional sources of pectin. Nature Publishing Group UK 2022-07-26 /pmc/articles/PMC9325980/ /pubmed/35882905 http://dx.doi.org/10.1038/s41598-022-16858-0 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Spinei, Mariana
Oroian, Mircea
Microwave-assisted extraction of pectin from grape pomace
title Microwave-assisted extraction of pectin from grape pomace
title_full Microwave-assisted extraction of pectin from grape pomace
title_fullStr Microwave-assisted extraction of pectin from grape pomace
title_full_unstemmed Microwave-assisted extraction of pectin from grape pomace
title_short Microwave-assisted extraction of pectin from grape pomace
title_sort microwave-assisted extraction of pectin from grape pomace
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9325980/
https://www.ncbi.nlm.nih.gov/pubmed/35882905
http://dx.doi.org/10.1038/s41598-022-16858-0
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