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Effects of Annealing and Thickness of Co(60)Fe(20)Yb(20) Nanofilms on Their Structure, Magnetic Properties, Electrical Efficiency, and Nanomechanical Characteristics

X-ray diffraction (XRD) analysis showed that metal oxide peaks appear at 2θ = 47.7°, 54.5°, and 56.3°, corresponding to Yb(2)O(3) (440), Co(2)O(3) (422), and Co(2)O(3) (511). It was found that oxide formation plays an important role in magnetic, electrical, and surface energy. For magnetic and elect...

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Autores principales: Liu, Wen-Jen, Chang, Yung-Huang, Chen, Yuan-Tsung, Chiu, Po-Chun, Guo, Jian-Cheng, Lin, Shih-Hung, Chi, Po-Wei
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9329774/
https://www.ncbi.nlm.nih.gov/pubmed/35897615
http://dx.doi.org/10.3390/ma15155184
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author Liu, Wen-Jen
Chang, Yung-Huang
Chen, Yuan-Tsung
Chiu, Po-Chun
Guo, Jian-Cheng
Lin, Shih-Hung
Chi, Po-Wei
author_facet Liu, Wen-Jen
Chang, Yung-Huang
Chen, Yuan-Tsung
Chiu, Po-Chun
Guo, Jian-Cheng
Lin, Shih-Hung
Chi, Po-Wei
author_sort Liu, Wen-Jen
collection PubMed
description X-ray diffraction (XRD) analysis showed that metal oxide peaks appear at 2θ = 47.7°, 54.5°, and 56.3°, corresponding to Yb(2)O(3) (440), Co(2)O(3) (422), and Co(2)O(3) (511). It was found that oxide formation plays an important role in magnetic, electrical, and surface energy. For magnetic and electrical measurements, the highest alternating current magnetic susceptibility (χ(ac)) and the lowest resistivity (×10(−2) Ω·cm) were 0.213 and 0.42, respectively, and at 50 nm, it annealed at 300 °C due to weak oxide formation. For mechanical measurement, the highest value of hardness was 15.93 GPa at 200 °C in a 50 nm thick film. When the thickness increased from 10 to 50 nm, the hardness and Young’s modulus of the Co(60)Fe(20)Yb(20) film also showed a saturation trend. After annealing at 300 °C, Co(60)Fe(20)Yb(20) films of 40 nm thickness showed the highest surface energy. Higher surface energy indicated stronger adhesion, allowing for the formation of multilayer thin films. The optimal condition was found to be 50 nm with annealing at 300 °C due to high χ(ac), strong adhesion, high nano-mechanical properties, and low resistivity.
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spelling pubmed-93297742022-07-29 Effects of Annealing and Thickness of Co(60)Fe(20)Yb(20) Nanofilms on Their Structure, Magnetic Properties, Electrical Efficiency, and Nanomechanical Characteristics Liu, Wen-Jen Chang, Yung-Huang Chen, Yuan-Tsung Chiu, Po-Chun Guo, Jian-Cheng Lin, Shih-Hung Chi, Po-Wei Materials (Basel) Article X-ray diffraction (XRD) analysis showed that metal oxide peaks appear at 2θ = 47.7°, 54.5°, and 56.3°, corresponding to Yb(2)O(3) (440), Co(2)O(3) (422), and Co(2)O(3) (511). It was found that oxide formation plays an important role in magnetic, electrical, and surface energy. For magnetic and electrical measurements, the highest alternating current magnetic susceptibility (χ(ac)) and the lowest resistivity (×10(−2) Ω·cm) were 0.213 and 0.42, respectively, and at 50 nm, it annealed at 300 °C due to weak oxide formation. For mechanical measurement, the highest value of hardness was 15.93 GPa at 200 °C in a 50 nm thick film. When the thickness increased from 10 to 50 nm, the hardness and Young’s modulus of the Co(60)Fe(20)Yb(20) film also showed a saturation trend. After annealing at 300 °C, Co(60)Fe(20)Yb(20) films of 40 nm thickness showed the highest surface energy. Higher surface energy indicated stronger adhesion, allowing for the formation of multilayer thin films. The optimal condition was found to be 50 nm with annealing at 300 °C due to high χ(ac), strong adhesion, high nano-mechanical properties, and low resistivity. MDPI 2022-07-26 /pmc/articles/PMC9329774/ /pubmed/35897615 http://dx.doi.org/10.3390/ma15155184 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Liu, Wen-Jen
Chang, Yung-Huang
Chen, Yuan-Tsung
Chiu, Po-Chun
Guo, Jian-Cheng
Lin, Shih-Hung
Chi, Po-Wei
Effects of Annealing and Thickness of Co(60)Fe(20)Yb(20) Nanofilms on Their Structure, Magnetic Properties, Electrical Efficiency, and Nanomechanical Characteristics
title Effects of Annealing and Thickness of Co(60)Fe(20)Yb(20) Nanofilms on Their Structure, Magnetic Properties, Electrical Efficiency, and Nanomechanical Characteristics
title_full Effects of Annealing and Thickness of Co(60)Fe(20)Yb(20) Nanofilms on Their Structure, Magnetic Properties, Electrical Efficiency, and Nanomechanical Characteristics
title_fullStr Effects of Annealing and Thickness of Co(60)Fe(20)Yb(20) Nanofilms on Their Structure, Magnetic Properties, Electrical Efficiency, and Nanomechanical Characteristics
title_full_unstemmed Effects of Annealing and Thickness of Co(60)Fe(20)Yb(20) Nanofilms on Their Structure, Magnetic Properties, Electrical Efficiency, and Nanomechanical Characteristics
title_short Effects of Annealing and Thickness of Co(60)Fe(20)Yb(20) Nanofilms on Their Structure, Magnetic Properties, Electrical Efficiency, and Nanomechanical Characteristics
title_sort effects of annealing and thickness of co(60)fe(20)yb(20) nanofilms on their structure, magnetic properties, electrical efficiency, and nanomechanical characteristics
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9329774/
https://www.ncbi.nlm.nih.gov/pubmed/35897615
http://dx.doi.org/10.3390/ma15155184
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