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Quantitative Analysis of Routine Chemical Constituents of Tobacco Based on Thermogravimetric Analysis

[Image: see text] As the most basic indexes to evaluate the quality of tobacco, the contents of routine chemical constituents in tobacco are mainly detected by continuous-flow analysis at present. However, this method suffers from complex operation, time consumption, and environmental pollution. Thu...

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Autores principales: Peng, Yuhan, Bi, Yiming, Dai, Lu, Li, Haifeng, Cao, Depo, Qi, Qijie, Liao, Fu, Zhang, Ke, Shen, Yudong, Du, Fangqi, Wang, Hui
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9352168/
https://www.ncbi.nlm.nih.gov/pubmed/35936416
http://dx.doi.org/10.1021/acsomega.2c02243
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author Peng, Yuhan
Bi, Yiming
Dai, Lu
Li, Haifeng
Cao, Depo
Qi, Qijie
Liao, Fu
Zhang, Ke
Shen, Yudong
Du, Fangqi
Wang, Hui
author_facet Peng, Yuhan
Bi, Yiming
Dai, Lu
Li, Haifeng
Cao, Depo
Qi, Qijie
Liao, Fu
Zhang, Ke
Shen, Yudong
Du, Fangqi
Wang, Hui
author_sort Peng, Yuhan
collection PubMed
description [Image: see text] As the most basic indexes to evaluate the quality of tobacco, the contents of routine chemical constituents in tobacco are mainly detected by continuous-flow analysis at present. However, this method suffers from complex operation, time consumption, and environmental pollution. Thus, it is necessary to establish a rapid accurate detection method. Herein, different from the ongoing research studies that mainly chose near-infrared spectroscopy as the information source for quantitative analysis of chemical components in tobacco, we proposed for the first time to use the thermogravimetric (TG) curve to characterize the chemical composition of tobacco. The quantitative analysis models of six routine chemical constituents in tobacco, including total sugar, reducing sugar, total nitrogen, total alkaloids, chlorine, and potassium, were established by the combination of TG curve and partial least squares algorithm. The accuracy of the model was confirmed by the value of root mean square error for prediction. The models can be used for the rapid accurate analysis of compound contents. Moreover, we performed an in-depth analysis of the chemical mechanism revealed by the result of the quantitative model, namely, the regression coefficient, which reflected the correlation degree between the six chemicals and different stages of the tobacco thermal decomposition process.
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spelling pubmed-93521682022-08-05 Quantitative Analysis of Routine Chemical Constituents of Tobacco Based on Thermogravimetric Analysis Peng, Yuhan Bi, Yiming Dai, Lu Li, Haifeng Cao, Depo Qi, Qijie Liao, Fu Zhang, Ke Shen, Yudong Du, Fangqi Wang, Hui ACS Omega [Image: see text] As the most basic indexes to evaluate the quality of tobacco, the contents of routine chemical constituents in tobacco are mainly detected by continuous-flow analysis at present. However, this method suffers from complex operation, time consumption, and environmental pollution. Thus, it is necessary to establish a rapid accurate detection method. Herein, different from the ongoing research studies that mainly chose near-infrared spectroscopy as the information source for quantitative analysis of chemical components in tobacco, we proposed for the first time to use the thermogravimetric (TG) curve to characterize the chemical composition of tobacco. The quantitative analysis models of six routine chemical constituents in tobacco, including total sugar, reducing sugar, total nitrogen, total alkaloids, chlorine, and potassium, were established by the combination of TG curve and partial least squares algorithm. The accuracy of the model was confirmed by the value of root mean square error for prediction. The models can be used for the rapid accurate analysis of compound contents. Moreover, we performed an in-depth analysis of the chemical mechanism revealed by the result of the quantitative model, namely, the regression coefficient, which reflected the correlation degree between the six chemicals and different stages of the tobacco thermal decomposition process. American Chemical Society 2022-07-21 /pmc/articles/PMC9352168/ /pubmed/35936416 http://dx.doi.org/10.1021/acsomega.2c02243 Text en © 2022 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by-nc-nd/4.0/Permits non-commercial access and re-use, provided that author attribution and integrity are maintained; but does not permit creation of adaptations or other derivative works (https://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Peng, Yuhan
Bi, Yiming
Dai, Lu
Li, Haifeng
Cao, Depo
Qi, Qijie
Liao, Fu
Zhang, Ke
Shen, Yudong
Du, Fangqi
Wang, Hui
Quantitative Analysis of Routine Chemical Constituents of Tobacco Based on Thermogravimetric Analysis
title Quantitative Analysis of Routine Chemical Constituents of Tobacco Based on Thermogravimetric Analysis
title_full Quantitative Analysis of Routine Chemical Constituents of Tobacco Based on Thermogravimetric Analysis
title_fullStr Quantitative Analysis of Routine Chemical Constituents of Tobacco Based on Thermogravimetric Analysis
title_full_unstemmed Quantitative Analysis of Routine Chemical Constituents of Tobacco Based on Thermogravimetric Analysis
title_short Quantitative Analysis of Routine Chemical Constituents of Tobacco Based on Thermogravimetric Analysis
title_sort quantitative analysis of routine chemical constituents of tobacco based on thermogravimetric analysis
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9352168/
https://www.ncbi.nlm.nih.gov/pubmed/35936416
http://dx.doi.org/10.1021/acsomega.2c02243
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