Growth of Pentacene Crystals by Naphthalene Flux Method

[Image: see text] We report the crystal growth of pentacene from a solution of naphthalene. The solubility of pentacene in naphthalene was evaluated by optical absorption at elevated temperature. The crystal growth was performed in an H-shaped sealed glass tube or metal vessels sealed with ultrahigh...

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Autores principales: Yang, Xiaoran, Li, Mingzhe, Maeno, Akira, Yanase, Takashi, Yokokura, Seiya, Nagahama, Taro, Shimada, Toshihiro
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9386793/
https://www.ncbi.nlm.nih.gov/pubmed/35990455
http://dx.doi.org/10.1021/acsomega.2c03551
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author Yang, Xiaoran
Li, Mingzhe
Maeno, Akira
Yanase, Takashi
Yokokura, Seiya
Nagahama, Taro
Shimada, Toshihiro
author_facet Yang, Xiaoran
Li, Mingzhe
Maeno, Akira
Yanase, Takashi
Yokokura, Seiya
Nagahama, Taro
Shimada, Toshihiro
author_sort Yang, Xiaoran
collection PubMed
description [Image: see text] We report the crystal growth of pentacene from a solution of naphthalene. The solubility of pentacene in naphthalene was evaluated by optical absorption at elevated temperature. The crystal growth was performed in an H-shaped sealed glass tube or metal vessels sealed with ultrahigh-vacuum compatible flanges placed in heated two-zone aluminum blocks. The obtained crystals had a single-crystal-like appearance and flat surface. They were made of aligned microtwins of the “bulk type” (interlayer spacing 14.5 Å) polymorph.
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spelling pubmed-93867932022-08-19 Growth of Pentacene Crystals by Naphthalene Flux Method Yang, Xiaoran Li, Mingzhe Maeno, Akira Yanase, Takashi Yokokura, Seiya Nagahama, Taro Shimada, Toshihiro ACS Omega [Image: see text] We report the crystal growth of pentacene from a solution of naphthalene. The solubility of pentacene in naphthalene was evaluated by optical absorption at elevated temperature. The crystal growth was performed in an H-shaped sealed glass tube or metal vessels sealed with ultrahigh-vacuum compatible flanges placed in heated two-zone aluminum blocks. The obtained crystals had a single-crystal-like appearance and flat surface. They were made of aligned microtwins of the “bulk type” (interlayer spacing 14.5 Å) polymorph. American Chemical Society 2022-08-02 /pmc/articles/PMC9386793/ /pubmed/35990455 http://dx.doi.org/10.1021/acsomega.2c03551 Text en © 2022 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by-nc-nd/4.0/Permits non-commercial access and re-use, provided that author attribution and integrity are maintained; but does not permit creation of adaptations or other derivative works (https://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Yang, Xiaoran
Li, Mingzhe
Maeno, Akira
Yanase, Takashi
Yokokura, Seiya
Nagahama, Taro
Shimada, Toshihiro
Growth of Pentacene Crystals by Naphthalene Flux Method
title Growth of Pentacene Crystals by Naphthalene Flux Method
title_full Growth of Pentacene Crystals by Naphthalene Flux Method
title_fullStr Growth of Pentacene Crystals by Naphthalene Flux Method
title_full_unstemmed Growth of Pentacene Crystals by Naphthalene Flux Method
title_short Growth of Pentacene Crystals by Naphthalene Flux Method
title_sort growth of pentacene crystals by naphthalene flux method
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9386793/
https://www.ncbi.nlm.nih.gov/pubmed/35990455
http://dx.doi.org/10.1021/acsomega.2c03551
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