Cargando…

Preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material

Rapid energy consumption stimulates the development of energy-saving materials. In this work, the L–S eutectic mixture used as a PCM was compounded with EP via vacuum adsorption to synthesize LS/EP CPCM. The maximum mass adsorption rate of EP on L–S is determined to be 70% via leakage experiments. T...

Descripción completa

Detalles Bibliográficos
Autores principales: Liu, Xuying, Zhao, Yunchao, Fan, Zhixuan, Shi, Yu, Jiang, Dahua
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9397110/
https://www.ncbi.nlm.nih.gov/pubmed/36093250
http://dx.doi.org/10.1039/d2ra02345h
_version_ 1784772062932369408
author Liu, Xuying
Zhao, Yunchao
Fan, Zhixuan
Shi, Yu
Jiang, Dahua
author_facet Liu, Xuying
Zhao, Yunchao
Fan, Zhixuan
Shi, Yu
Jiang, Dahua
author_sort Liu, Xuying
collection PubMed
description Rapid energy consumption stimulates the development of energy-saving materials. In this work, the L–S eutectic mixture used as a PCM was compounded with EP via vacuum adsorption to synthesize LS/EP CPCM. The maximum mass adsorption rate of EP on L–S is determined to be 70% via leakage experiments. The microscopic morphology, chemical, and crystal structure were characterized using scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), and X-ray diffraction (XRD), respectively. The phase change properties were measured by differential scanning calorimetry (DSC). The melting temperature of LS/EP is 37.79 °C, with a latent heat of 126.05 J g(−1), and it has a crystallinity of over 90%. The thermal decomposition was evaluated by TGA. The initial decomposition temperature is 132.20 °C for LS/EP. In addition, the results of accelerated phase change cycling experiments showed that LS/EP CPCM has good reliability.
format Online
Article
Text
id pubmed-9397110
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher The Royal Society of Chemistry
record_format MEDLINE/PubMed
spelling pubmed-93971102022-09-08 Preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material Liu, Xuying Zhao, Yunchao Fan, Zhixuan Shi, Yu Jiang, Dahua RSC Adv Chemistry Rapid energy consumption stimulates the development of energy-saving materials. In this work, the L–S eutectic mixture used as a PCM was compounded with EP via vacuum adsorption to synthesize LS/EP CPCM. The maximum mass adsorption rate of EP on L–S is determined to be 70% via leakage experiments. The microscopic morphology, chemical, and crystal structure were characterized using scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), and X-ray diffraction (XRD), respectively. The phase change properties were measured by differential scanning calorimetry (DSC). The melting temperature of LS/EP is 37.79 °C, with a latent heat of 126.05 J g(−1), and it has a crystallinity of over 90%. The thermal decomposition was evaluated by TGA. The initial decomposition temperature is 132.20 °C for LS/EP. In addition, the results of accelerated phase change cycling experiments showed that LS/EP CPCM has good reliability. The Royal Society of Chemistry 2022-08-23 /pmc/articles/PMC9397110/ /pubmed/36093250 http://dx.doi.org/10.1039/d2ra02345h Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/
spellingShingle Chemistry
Liu, Xuying
Zhao, Yunchao
Fan, Zhixuan
Shi, Yu
Jiang, Dahua
Preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material
title Preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material
title_full Preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material
title_fullStr Preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material
title_full_unstemmed Preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material
title_short Preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material
title_sort preparation and characterization of lauric acid–stearic acid/expanded perlite as a composite phase change material
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9397110/
https://www.ncbi.nlm.nih.gov/pubmed/36093250
http://dx.doi.org/10.1039/d2ra02345h
work_keys_str_mv AT liuxuying preparationandcharacterizationoflauricacidstearicacidexpandedperliteasacompositephasechangematerial
AT zhaoyunchao preparationandcharacterizationoflauricacidstearicacidexpandedperliteasacompositephasechangematerial
AT fanzhixuan preparationandcharacterizationoflauricacidstearicacidexpandedperliteasacompositephasechangematerial
AT shiyu preparationandcharacterizationoflauricacidstearicacidexpandedperliteasacompositephasechangematerial
AT jiangdahua preparationandcharacterizationoflauricacidstearicacidexpandedperliteasacompositephasechangematerial