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Protocol for fabrication and characterization of Fe-SAC@COF for electrocatalytic oxygen evolution reaction

Single-atom catalysts (SACs) have promising atomic utilization efficiency and catalytic activity, but their construction with a specific coordination mode remains challenging. This protocol describes the synthesis of a coordinated Fe-SAC@COF for boosted electrocatalytic oxygen evolution reaction (OE...

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Detalles Bibliográficos
Autores principales: Wang, Xiao, Zhou, Wei, Wu, Hao, Deng, Wei-Qiao
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9405112/
https://www.ncbi.nlm.nih.gov/pubmed/36035801
http://dx.doi.org/10.1016/j.xpro.2022.101626
Descripción
Sumario:Single-atom catalysts (SACs) have promising atomic utilization efficiency and catalytic activity, but their construction with a specific coordination mode remains challenging. This protocol describes the synthesis of a coordinated Fe-SAC@COF for boosted electrocatalytic oxygen evolution reaction (OER). We also detail the steps for single iron atoms confinement and characterization of the COF and Fe-SAC@COF with X-ray diffraction and transmission electron microscopy technique. For complete details on the use and execution of this protocol, please refer to Wang et al. (2022).