A Convenient, Rapid, Conventional Heating Route to MIDA Boronates

A cheap, conventional, sealed heating reactor proved to be a useful alternative to a microwave reactor in the synthesis of a >20-member MIDA boronate library (MIDA = N-methyliminodiacetic acid). Reaction times were 10 min and work-ups were minimal, saving on energy and solvent usage.

Detalles Bibliográficos
Autores principales: McGown, Andrew, Edmonds, Anthony K., Guest, Daniel, Holmes, Verity L., Dadswell, Chris, González-Méndez, Ramón, Goodall, Charles A. I., Bagley, Mark C., Greenland, Barnaby W., Spencer, John
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9414357/
https://www.ncbi.nlm.nih.gov/pubmed/36014293
http://dx.doi.org/10.3390/molecules27165052
Descripción
Sumario:A cheap, conventional, sealed heating reactor proved to be a useful alternative to a microwave reactor in the synthesis of a >20-member MIDA boronate library (MIDA = N-methyliminodiacetic acid). Reaction times were 10 min and work-ups were minimal, saving on energy and solvent usage.

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