A Convenient, Rapid, Conventional Heating Route to MIDA Boronates

A cheap, conventional, sealed heating reactor proved to be a useful alternative to a microwave reactor in the synthesis of a >20-member MIDA boronate library (MIDA = N-methyliminodiacetic acid). Reaction times were 10 min and work-ups were minimal, saving on energy and solvent usage.

Detalles Bibliográficos
Autores principales: McGown, Andrew, Edmonds, Anthony K., Guest, Daniel, Holmes, Verity L., Dadswell, Chris, González-Méndez, Ramón, Goodall, Charles A. I., Bagley, Mark C., Greenland, Barnaby W., Spencer, John
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9414357/
https://www.ncbi.nlm.nih.gov/pubmed/36014293
http://dx.doi.org/10.3390/molecules27165052
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author McGown, Andrew
Edmonds, Anthony K.
Guest, Daniel
Holmes, Verity L.
Dadswell, Chris
González-Méndez, Ramón
Goodall, Charles A. I.
Bagley, Mark C.
Greenland, Barnaby W.
Spencer, John
author_facet McGown, Andrew
Edmonds, Anthony K.
Guest, Daniel
Holmes, Verity L.
Dadswell, Chris
González-Méndez, Ramón
Goodall, Charles A. I.
Bagley, Mark C.
Greenland, Barnaby W.
Spencer, John
author_sort McGown, Andrew
collection PubMed
description A cheap, conventional, sealed heating reactor proved to be a useful alternative to a microwave reactor in the synthesis of a >20-member MIDA boronate library (MIDA = N-methyliminodiacetic acid). Reaction times were 10 min and work-ups were minimal, saving on energy and solvent usage.
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spelling pubmed-94143572022-08-27 A Convenient, Rapid, Conventional Heating Route to MIDA Boronates McGown, Andrew Edmonds, Anthony K. Guest, Daniel Holmes, Verity L. Dadswell, Chris González-Méndez, Ramón Goodall, Charles A. I. Bagley, Mark C. Greenland, Barnaby W. Spencer, John Molecules Article A cheap, conventional, sealed heating reactor proved to be a useful alternative to a microwave reactor in the synthesis of a >20-member MIDA boronate library (MIDA = N-methyliminodiacetic acid). Reaction times were 10 min and work-ups were minimal, saving on energy and solvent usage. MDPI 2022-08-09 /pmc/articles/PMC9414357/ /pubmed/36014293 http://dx.doi.org/10.3390/molecules27165052 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
McGown, Andrew
Edmonds, Anthony K.
Guest, Daniel
Holmes, Verity L.
Dadswell, Chris
González-Méndez, Ramón
Goodall, Charles A. I.
Bagley, Mark C.
Greenland, Barnaby W.
Spencer, John
A Convenient, Rapid, Conventional Heating Route to MIDA Boronates
title A Convenient, Rapid, Conventional Heating Route to MIDA Boronates
title_full A Convenient, Rapid, Conventional Heating Route to MIDA Boronates
title_fullStr A Convenient, Rapid, Conventional Heating Route to MIDA Boronates
title_full_unstemmed A Convenient, Rapid, Conventional Heating Route to MIDA Boronates
title_short A Convenient, Rapid, Conventional Heating Route to MIDA Boronates
title_sort convenient, rapid, conventional heating route to mida boronates
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9414357/
https://www.ncbi.nlm.nih.gov/pubmed/36014293
http://dx.doi.org/10.3390/molecules27165052
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