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Isothermal Quenching of As-Cast Medium Carbon, High-Silicon AR Steel

Medium carbon high-silicon abrasion resistant (AR) steel was examined by performing dilatometry, light optical microscopy (LOM), scanning electron microscopy (SEM), and hardness measurements after isothermal bainitization and modified martempering and compared to direct quenching technology. A comme...

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Autores principales: Klančnik, Grega, Krajnc, Luka, Nagode, Aleš, Burja, Jaka
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9415478/
https://www.ncbi.nlm.nih.gov/pubmed/36013731
http://dx.doi.org/10.3390/ma15165595
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author Klančnik, Grega
Krajnc, Luka
Nagode, Aleš
Burja, Jaka
author_facet Klančnik, Grega
Krajnc, Luka
Nagode, Aleš
Burja, Jaka
author_sort Klančnik, Grega
collection PubMed
description Medium carbon high-silicon abrasion resistant (AR) steel was examined by performing dilatometry, light optical microscopy (LOM), scanning electron microscopy (SEM), and hardness measurements after isothermal bainitization and modified martempering and compared to direct quenching technology. A commercial thermodynamic tool was used for hardness prediction and compared to the measured one and revealed a rather good agreement for direct quenching, as was the case for isothermal holdings near to the martensite start (Ms). The predicted martensite start temperatures were in good agreement with the experimental data, the experimental value was 321 °C, while the predicted values were 324 and 296 °C. However, a higher discrepancy appeared for isothermal holding much above the martensite transition in the bainite region resulting in lower measured hardness compared to the predictions related to the actual kinetics and complexity of the formed final volume percentages of phase constituents such as bainite, martensite, and rest austenite, later as a part of unfinished bainite transformation at studied temperature. The predicted hardness values for quenching, isothermal holding at 280, 300 and 350 °C were 50.6, 50.6, 49.4 and 49.4 HRC, while the measured values were 53.3, 48.3, 48 and 43 HRC, respectively. A very good agreement between the thermodynamic prediction was achieved by comparing the measured Ms concerning prior austenite grain size as one of the crucial parameters for setting a proper heat treatment strategy of various isothermal quenchings making thermodynamic predictions for low alloyed steels a powerful tool for optimizing the heat-treating operations.
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spelling pubmed-94154782022-08-27 Isothermal Quenching of As-Cast Medium Carbon, High-Silicon AR Steel Klančnik, Grega Krajnc, Luka Nagode, Aleš Burja, Jaka Materials (Basel) Article Medium carbon high-silicon abrasion resistant (AR) steel was examined by performing dilatometry, light optical microscopy (LOM), scanning electron microscopy (SEM), and hardness measurements after isothermal bainitization and modified martempering and compared to direct quenching technology. A commercial thermodynamic tool was used for hardness prediction and compared to the measured one and revealed a rather good agreement for direct quenching, as was the case for isothermal holdings near to the martensite start (Ms). The predicted martensite start temperatures were in good agreement with the experimental data, the experimental value was 321 °C, while the predicted values were 324 and 296 °C. However, a higher discrepancy appeared for isothermal holding much above the martensite transition in the bainite region resulting in lower measured hardness compared to the predictions related to the actual kinetics and complexity of the formed final volume percentages of phase constituents such as bainite, martensite, and rest austenite, later as a part of unfinished bainite transformation at studied temperature. The predicted hardness values for quenching, isothermal holding at 280, 300 and 350 °C were 50.6, 50.6, 49.4 and 49.4 HRC, while the measured values were 53.3, 48.3, 48 and 43 HRC, respectively. A very good agreement between the thermodynamic prediction was achieved by comparing the measured Ms concerning prior austenite grain size as one of the crucial parameters for setting a proper heat treatment strategy of various isothermal quenchings making thermodynamic predictions for low alloyed steels a powerful tool for optimizing the heat-treating operations. MDPI 2022-08-15 /pmc/articles/PMC9415478/ /pubmed/36013731 http://dx.doi.org/10.3390/ma15165595 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Klančnik, Grega
Krajnc, Luka
Nagode, Aleš
Burja, Jaka
Isothermal Quenching of As-Cast Medium Carbon, High-Silicon AR Steel
title Isothermal Quenching of As-Cast Medium Carbon, High-Silicon AR Steel
title_full Isothermal Quenching of As-Cast Medium Carbon, High-Silicon AR Steel
title_fullStr Isothermal Quenching of As-Cast Medium Carbon, High-Silicon AR Steel
title_full_unstemmed Isothermal Quenching of As-Cast Medium Carbon, High-Silicon AR Steel
title_short Isothermal Quenching of As-Cast Medium Carbon, High-Silicon AR Steel
title_sort isothermal quenching of as-cast medium carbon, high-silicon ar steel
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9415478/
https://www.ncbi.nlm.nih.gov/pubmed/36013731
http://dx.doi.org/10.3390/ma15165595
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