Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy

A significant electron-beam induced heating effect is demonstrated for liquid-phase transmission electron microscopy at low electron flux densities using Au nanoparticles as local nanothermometers. The obtained results are in agreement with theoretical considerations. Furthermore, the impact of beam...

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Detalles Bibliográficos
Autores principales: Fritsch, Birk, Hutzler, Andreas, Wu, Mingjian, Khadivianazar, Saba, Vogl, Lilian, Jank, Michael P. M., März, Martin, Spiecker, Erdmann
Formato: Online Artículo Texto
Lenguaje:English
Publicado: RSC 2021
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9419575/
https://www.ncbi.nlm.nih.gov/pubmed/36134158
http://dx.doi.org/10.1039/d0na01027h
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author Fritsch, Birk
Hutzler, Andreas
Wu, Mingjian
Khadivianazar, Saba
Vogl, Lilian
Jank, Michael P. M.
März, Martin
Spiecker, Erdmann
author_facet Fritsch, Birk
Hutzler, Andreas
Wu, Mingjian
Khadivianazar, Saba
Vogl, Lilian
Jank, Michael P. M.
März, Martin
Spiecker, Erdmann
author_sort Fritsch, Birk
collection PubMed
description A significant electron-beam induced heating effect is demonstrated for liquid-phase transmission electron microscopy at low electron flux densities using Au nanoparticles as local nanothermometers. The obtained results are in agreement with theoretical considerations. Furthermore, the impact of beam-induced heating on radiolysis chemistry is estimated and the consequences of the effect are discussed.
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spelling pubmed-94195752022-09-20 Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy Fritsch, Birk Hutzler, Andreas Wu, Mingjian Khadivianazar, Saba Vogl, Lilian Jank, Michael P. M. März, Martin Spiecker, Erdmann Nanoscale Adv Chemistry A significant electron-beam induced heating effect is demonstrated for liquid-phase transmission electron microscopy at low electron flux densities using Au nanoparticles as local nanothermometers. The obtained results are in agreement with theoretical considerations. Furthermore, the impact of beam-induced heating on radiolysis chemistry is estimated and the consequences of the effect are discussed. RSC 2021-02-19 /pmc/articles/PMC9419575/ /pubmed/36134158 http://dx.doi.org/10.1039/d0na01027h Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by/3.0/
spellingShingle Chemistry
Fritsch, Birk
Hutzler, Andreas
Wu, Mingjian
Khadivianazar, Saba
Vogl, Lilian
Jank, Michael P. M.
März, Martin
Spiecker, Erdmann
Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy
title Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy
title_full Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy
title_fullStr Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy
title_full_unstemmed Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy
title_short Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy
title_sort accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9419575/
https://www.ncbi.nlm.nih.gov/pubmed/36134158
http://dx.doi.org/10.1039/d0na01027h
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