Crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4H-benzo[def]carbazol-4-yl]ethan-1-one

The crystal of the title compound, C(60)H(38)N(2)O(2), which crystallizes in the monoclinic space group P2(1)/n, was obtained by thermal evaporation of a 1:1 di­chloro­methane and hexa­nes solution of the pure compound. The crystal structure is stabilized by π–π inter­actions between benzo[def]carba...

Descripción completa

Detalles Bibliográficos
Autores principales: Hsiao, Huan-Chang, Chen, Pei-Lin, Chuang, Shih-Ching
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2022
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9431799/
https://www.ncbi.nlm.nih.gov/pubmed/36072156
http://dx.doi.org/10.1107/S2056989022004509
_version_ 1784780154275364864
author Hsiao, Huan-Chang
Chen, Pei-Lin
Chuang, Shih-Ching
author_facet Hsiao, Huan-Chang
Chen, Pei-Lin
Chuang, Shih-Ching
author_sort Hsiao, Huan-Chang
collection PubMed
description The crystal of the title compound, C(60)H(38)N(2)O(2), which crystallizes in the monoclinic space group P2(1)/n, was obtained by thermal evaporation of a 1:1 di­chloro­methane and hexa­nes solution of the pure compound. The crystal structure is stabilized by π–π inter­actions between benzo[def]carbazole moieties and carbon­yl–carbonyl inter­actions between the two acetyl groups.
format Online
Article
Text
id pubmed-9431799
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-94317992022-09-06 Crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4H-benzo[def]carbazol-4-yl]ethan-1-one Hsiao, Huan-Chang Chen, Pei-Lin Chuang, Shih-Ching Acta Crystallogr E Crystallogr Commun Research Communications The crystal of the title compound, C(60)H(38)N(2)O(2), which crystallizes in the monoclinic space group P2(1)/n, was obtained by thermal evaporation of a 1:1 di­chloro­methane and hexa­nes solution of the pure compound. The crystal structure is stabilized by π–π inter­actions between benzo[def]carbazole moieties and carbon­yl–carbonyl inter­actions between the two acetyl groups. International Union of Crystallography 2022-05-13 /pmc/articles/PMC9431799/ /pubmed/36072156 http://dx.doi.org/10.1107/S2056989022004509 Text en © Hsiao et al. 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Hsiao, Huan-Chang
Chen, Pei-Lin
Chuang, Shih-Ching
Crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4H-benzo[def]carbazol-4-yl]ethan-1-one
title Crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4H-benzo[def]carbazol-4-yl]ethan-1-one
title_full Crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4H-benzo[def]carbazol-4-yl]ethan-1-one
title_fullStr Crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4H-benzo[def]carbazol-4-yl]ethan-1-one
title_full_unstemmed Crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4H-benzo[def]carbazol-4-yl]ethan-1-one
title_short Crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4H-benzo[def]carbazol-4-yl]ethan-1-one
title_sort crystal structure and fluorescence of 1-[8-phenyl-9-(phenyl­ethyn­yl)-4h-benzo[def]carbazol-4-yl]ethan-1-one
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9431799/
https://www.ncbi.nlm.nih.gov/pubmed/36072156
http://dx.doi.org/10.1107/S2056989022004509
work_keys_str_mv AT hsiaohuanchang crystalstructureandfluorescenceof18phenyl9phenylethynyl4hbenzodefcarbazol4ylethan1one
AT chenpeilin crystalstructureandfluorescenceof18phenyl9phenylethynyl4hbenzodefcarbazol4ylethan1one
AT chuangshihching crystalstructureandfluorescenceof18phenyl9phenylethynyl4hbenzodefcarbazol4ylethan1one

Ejemplares similares