Cargando…

SnapFib: An easy build Arduino based tabletop prototype for thin film deposition by Successive Ionic Layer Adsorption and Reaction method

Non-vacuum-based techniques are suitable for thin-film deposition with precision stoichiometric control. Among those, the Successive Ionic Layer Adsorption and Reaction (SILAR) method is gaining popularity for its aqueous-based almost room temperature deposition option. This method has many advantag...

Descripción completa

Detalles Bibliográficos
Autores principales: Sen Gupta, Ashoke Kumar, Adnan, Abu, Bhattacharjee, Shantanu, Das, Nipu Kumar, Matin, M.A., Quamruzzaman, Muhammad
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9436813/
https://www.ncbi.nlm.nih.gov/pubmed/36062212
http://dx.doi.org/10.1016/j.ohx.2022.e00347
_version_ 1784781456169500672
author Sen Gupta, Ashoke Kumar
Adnan, Abu
Bhattacharjee, Shantanu
Das, Nipu Kumar
Matin, M.A.
Quamruzzaman, Muhammad
author_facet Sen Gupta, Ashoke Kumar
Adnan, Abu
Bhattacharjee, Shantanu
Das, Nipu Kumar
Matin, M.A.
Quamruzzaman, Muhammad
author_sort Sen Gupta, Ashoke Kumar
collection PubMed
description Non-vacuum-based techniques are suitable for thin-film deposition with precision stoichiometric control. Among those, the Successive Ionic Layer Adsorption and Reaction (SILAR) method is gaining popularity for its aqueous-based almost room temperature deposition option. This method has many advantages, including the ability to control the elemental composition and stoichiometry of precursors. It is also suitable for large-area deposition. It has many runtime parameters, e.g., the number of cycles, dip time, rinse time, etc., that control the quantitative and qualitative physical properties of the deposited film. But manually controlling all these parameters for the whole process is very difficult and cumbersome. Although there are several reports published on this similar type of home-built prototype, for fast, accurate, and economically affordable deposition operations, we need to develop a machine that maintains all the properties of the SILAR process and can be made using cheap technologies. Here we report the SnapFib, a cost-effective automated tabletop prototype machine that is easy to build for thin-film deposition on soda-lime glass substrates by the SILAR method without almost any human intervention. SnapFib is built using linear actuators, an ATmega328P (a microcontroller available on Arduino boards), and some other parts collected from laboratory sites. The whole firmware needed for this device has been developed and maintained using the Arduino IDE (Integrated Development Environment). All required functional features and control parameters are encoded in the microcontroller firmware. The construction cost of this prototype is around 600 USD. We validated our construction through XRD (X-ray Diffraction) and FESEM (Field Emission Scanning Electron Microscope) characterizations of thin films that were deposited by SnapFib. Since this is built under the CC-BY license, students and researchers can freely perform and validate their experiments and modify the hardware and software as required. With how easy it is to make and how much it costs; we hope that many thin-film deposition labs will quickly start using SnapFib as an added benefit.
format Online
Article
Text
id pubmed-9436813
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher Elsevier
record_format MEDLINE/PubMed
spelling pubmed-94368132022-09-03 SnapFib: An easy build Arduino based tabletop prototype for thin film deposition by Successive Ionic Layer Adsorption and Reaction method Sen Gupta, Ashoke Kumar Adnan, Abu Bhattacharjee, Shantanu Das, Nipu Kumar Matin, M.A. Quamruzzaman, Muhammad HardwareX Article Non-vacuum-based techniques are suitable for thin-film deposition with precision stoichiometric control. Among those, the Successive Ionic Layer Adsorption and Reaction (SILAR) method is gaining popularity for its aqueous-based almost room temperature deposition option. This method has many advantages, including the ability to control the elemental composition and stoichiometry of precursors. It is also suitable for large-area deposition. It has many runtime parameters, e.g., the number of cycles, dip time, rinse time, etc., that control the quantitative and qualitative physical properties of the deposited film. But manually controlling all these parameters for the whole process is very difficult and cumbersome. Although there are several reports published on this similar type of home-built prototype, for fast, accurate, and economically affordable deposition operations, we need to develop a machine that maintains all the properties of the SILAR process and can be made using cheap technologies. Here we report the SnapFib, a cost-effective automated tabletop prototype machine that is easy to build for thin-film deposition on soda-lime glass substrates by the SILAR method without almost any human intervention. SnapFib is built using linear actuators, an ATmega328P (a microcontroller available on Arduino boards), and some other parts collected from laboratory sites. The whole firmware needed for this device has been developed and maintained using the Arduino IDE (Integrated Development Environment). All required functional features and control parameters are encoded in the microcontroller firmware. The construction cost of this prototype is around 600 USD. We validated our construction through XRD (X-ray Diffraction) and FESEM (Field Emission Scanning Electron Microscope) characterizations of thin films that were deposited by SnapFib. Since this is built under the CC-BY license, students and researchers can freely perform and validate their experiments and modify the hardware and software as required. With how easy it is to make and how much it costs; we hope that many thin-film deposition labs will quickly start using SnapFib as an added benefit. Elsevier 2022-08-19 /pmc/articles/PMC9436813/ /pubmed/36062212 http://dx.doi.org/10.1016/j.ohx.2022.e00347 Text en © 2022 The Author(s) https://creativecommons.org/licenses/by/4.0/This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Sen Gupta, Ashoke Kumar
Adnan, Abu
Bhattacharjee, Shantanu
Das, Nipu Kumar
Matin, M.A.
Quamruzzaman, Muhammad
SnapFib: An easy build Arduino based tabletop prototype for thin film deposition by Successive Ionic Layer Adsorption and Reaction method
title SnapFib: An easy build Arduino based tabletop prototype for thin film deposition by Successive Ionic Layer Adsorption and Reaction method
title_full SnapFib: An easy build Arduino based tabletop prototype for thin film deposition by Successive Ionic Layer Adsorption and Reaction method
title_fullStr SnapFib: An easy build Arduino based tabletop prototype for thin film deposition by Successive Ionic Layer Adsorption and Reaction method
title_full_unstemmed SnapFib: An easy build Arduino based tabletop prototype for thin film deposition by Successive Ionic Layer Adsorption and Reaction method
title_short SnapFib: An easy build Arduino based tabletop prototype for thin film deposition by Successive Ionic Layer Adsorption and Reaction method
title_sort snapfib: an easy build arduino based tabletop prototype for thin film deposition by successive ionic layer adsorption and reaction method
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9436813/
https://www.ncbi.nlm.nih.gov/pubmed/36062212
http://dx.doi.org/10.1016/j.ohx.2022.e00347
work_keys_str_mv AT senguptaashokekumar snapfibaneasybuildarduinobasedtabletopprototypeforthinfilmdepositionbysuccessiveioniclayeradsorptionandreactionmethod
AT adnanabu snapfibaneasybuildarduinobasedtabletopprototypeforthinfilmdepositionbysuccessiveioniclayeradsorptionandreactionmethod
AT bhattacharjeeshantanu snapfibaneasybuildarduinobasedtabletopprototypeforthinfilmdepositionbysuccessiveioniclayeradsorptionandreactionmethod
AT dasnipukumar snapfibaneasybuildarduinobasedtabletopprototypeforthinfilmdepositionbysuccessiveioniclayeradsorptionandreactionmethod
AT matinma snapfibaneasybuildarduinobasedtabletopprototypeforthinfilmdepositionbysuccessiveioniclayeradsorptionandreactionmethod
AT quamruzzamanmuhammad snapfibaneasybuildarduinobasedtabletopprototypeforthinfilmdepositionbysuccessiveioniclayeradsorptionandreactionmethod