Cargando…
Ti64/20Ag Porous Composites Fabricated by Powder Metallurgy for Biomedical Applications
We present a novel Ti64/20Ag highly porous composite fabricated by powder metallurgy for biomedical applications and provide an insight into its microstructure and mechanical proprieties. In this work, the Ti64/20Ag highly porous composites were successfully fabricated by the space holder technique...
Autores principales: | , , , , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9457260/ https://www.ncbi.nlm.nih.gov/pubmed/36079338 http://dx.doi.org/10.3390/ma15175956 |
_version_ | 1784786011872559104 |
---|---|
author | Olmos, Luis Gonzaléz-Pedraza, Ana S. Vergara-Hernández, Héctor J. Chávez, Jorge Jimenez, Omar Mihalcea, Elena Arteaga, Dante Ruiz-Mondragón, José J. |
author_facet | Olmos, Luis Gonzaléz-Pedraza, Ana S. Vergara-Hernández, Héctor J. Chávez, Jorge Jimenez, Omar Mihalcea, Elena Arteaga, Dante Ruiz-Mondragón, José J. |
author_sort | Olmos, Luis |
collection | PubMed |
description | We present a novel Ti64/20Ag highly porous composite fabricated by powder metallurgy for biomedical applications and provide an insight into its microstructure and mechanical proprieties. In this work, the Ti64/20Ag highly porous composites were successfully fabricated by the space holder technique and consolidated by liquid phase sintering, at lower temperatures than the ones used for Ti64 materials. The sintering densification was evaluated by dilatometry tests and the microstructural characterization and porosity features were determined by scanning electron microscopy and computed microtomography. Permeability was estimated by numerical simulations on the 3D real microstructure. Mechanical properties were evaluated by simple compression tests. Densification was achieved by interparticle pore filling with liquid Ag that does not drain to the large pores, with additional densification due to the macroscopical deformation of large pores. Pore characteristics are closely linked to the pore formers and the permeability was highly increased by increasing the pore volume fraction, mainly because the connectivity was improved. As expected, with the increase in porosity, the mechanical properties decreased. These results permitted us to gain a greater understanding of the microstructure and to confirm that we developed a promising Ti64/20Ag composite, showing E of 7.4 GPa, σ(y) of 123 MPa and permeability of 3.93 × 10(−11) m(2). Enhanced adaptability and antibacterial proprieties due to Ag were obtained for bone implant applications. |
format | Online Article Text |
id | pubmed-9457260 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-94572602022-09-09 Ti64/20Ag Porous Composites Fabricated by Powder Metallurgy for Biomedical Applications Olmos, Luis Gonzaléz-Pedraza, Ana S. Vergara-Hernández, Héctor J. Chávez, Jorge Jimenez, Omar Mihalcea, Elena Arteaga, Dante Ruiz-Mondragón, José J. Materials (Basel) Article We present a novel Ti64/20Ag highly porous composite fabricated by powder metallurgy for biomedical applications and provide an insight into its microstructure and mechanical proprieties. In this work, the Ti64/20Ag highly porous composites were successfully fabricated by the space holder technique and consolidated by liquid phase sintering, at lower temperatures than the ones used for Ti64 materials. The sintering densification was evaluated by dilatometry tests and the microstructural characterization and porosity features were determined by scanning electron microscopy and computed microtomography. Permeability was estimated by numerical simulations on the 3D real microstructure. Mechanical properties were evaluated by simple compression tests. Densification was achieved by interparticle pore filling with liquid Ag that does not drain to the large pores, with additional densification due to the macroscopical deformation of large pores. Pore characteristics are closely linked to the pore formers and the permeability was highly increased by increasing the pore volume fraction, mainly because the connectivity was improved. As expected, with the increase in porosity, the mechanical properties decreased. These results permitted us to gain a greater understanding of the microstructure and to confirm that we developed a promising Ti64/20Ag composite, showing E of 7.4 GPa, σ(y) of 123 MPa and permeability of 3.93 × 10(−11) m(2). Enhanced adaptability and antibacterial proprieties due to Ag were obtained for bone implant applications. MDPI 2022-08-29 /pmc/articles/PMC9457260/ /pubmed/36079338 http://dx.doi.org/10.3390/ma15175956 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Olmos, Luis Gonzaléz-Pedraza, Ana S. Vergara-Hernández, Héctor J. Chávez, Jorge Jimenez, Omar Mihalcea, Elena Arteaga, Dante Ruiz-Mondragón, José J. Ti64/20Ag Porous Composites Fabricated by Powder Metallurgy for Biomedical Applications |
title | Ti64/20Ag Porous Composites Fabricated by Powder Metallurgy for Biomedical Applications |
title_full | Ti64/20Ag Porous Composites Fabricated by Powder Metallurgy for Biomedical Applications |
title_fullStr | Ti64/20Ag Porous Composites Fabricated by Powder Metallurgy for Biomedical Applications |
title_full_unstemmed | Ti64/20Ag Porous Composites Fabricated by Powder Metallurgy for Biomedical Applications |
title_short | Ti64/20Ag Porous Composites Fabricated by Powder Metallurgy for Biomedical Applications |
title_sort | ti64/20ag porous composites fabricated by powder metallurgy for biomedical applications |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9457260/ https://www.ncbi.nlm.nih.gov/pubmed/36079338 http://dx.doi.org/10.3390/ma15175956 |
work_keys_str_mv | AT olmosluis ti6420agporouscompositesfabricatedbypowdermetallurgyforbiomedicalapplications AT gonzalezpedrazaanas ti6420agporouscompositesfabricatedbypowdermetallurgyforbiomedicalapplications AT vergarahernandezhectorj ti6420agporouscompositesfabricatedbypowdermetallurgyforbiomedicalapplications AT chavezjorge ti6420agporouscompositesfabricatedbypowdermetallurgyforbiomedicalapplications AT jimenezomar ti6420agporouscompositesfabricatedbypowdermetallurgyforbiomedicalapplications AT mihalceaelena ti6420agporouscompositesfabricatedbypowdermetallurgyforbiomedicalapplications AT arteagadante ti6420agporouscompositesfabricatedbypowdermetallurgyforbiomedicalapplications AT ruizmondragonjosej ti6420agporouscompositesfabricatedbypowdermetallurgyforbiomedicalapplications |