Bis(oxotremorine) fumarate bis­(fumaric acid)

The title compound, bis­(oxotremorine) fumarate bis­(fumaric acid) {systematic name: 1-[4-(2-oxopyrrolidin-1-yl)but-2-yn­yl]pyrrolidinium (2E)-but-2-ene­di­o­ate bis­[(2E)-but-2-enedioic acid]}, 2C(12)H(19)N(2)O(+)·C(4)H(2)O(4) (2−)·2C(4)H(4)O(4), has a single oxotremorine monocation protonated at t...

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Detalles Bibliográficos
Autores principales: Naeem, Marilyn, Chadeayne, Andrew R., Golen, James A., Manke, David R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2022
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462024/
https://www.ncbi.nlm.nih.gov/pubmed/36337690
http://dx.doi.org/10.1107/S2414314622003649
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author Naeem, Marilyn
Chadeayne, Andrew R.
Golen, James A.
Manke, David R.
author_facet Naeem, Marilyn
Chadeayne, Andrew R.
Golen, James A.
Manke, David R.
author_sort Naeem, Marilyn
collection PubMed
description The title compound, bis­(oxotremorine) fumarate bis­(fumaric acid) {systematic name: 1-[4-(2-oxopyrrolidin-1-yl)but-2-yn­yl]pyrrolidinium (2E)-but-2-ene­di­o­ate bis­[(2E)-but-2-enedioic acid]}, 2C(12)H(19)N(2)O(+)·C(4)H(2)O(4) (2−)·2C(4)H(4)O(4), has a single oxotremorine monocation protonated at the pyrrolidine nitro­gen, one fumaric acid mol­ecule and half of a fumarate dianion in the asymmetric unit. The ions and fumaric acid mol­ecules are held together by N—H⋯O and O–H-⋯O hydrogen bonds in 40-membered rings with graph-set notation R (6) (6)(40). The fumarate ions join these rings into infinite chains along [001]. [Image: see text]
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spelling pubmed-94620242022-11-04 Bis(oxotremorine) fumarate bis­(fumaric acid) Naeem, Marilyn Chadeayne, Andrew R. Golen, James A. Manke, David R. IUCrdata Data Reports The title compound, bis­(oxotremorine) fumarate bis­(fumaric acid) {systematic name: 1-[4-(2-oxopyrrolidin-1-yl)but-2-yn­yl]pyrrolidinium (2E)-but-2-ene­di­o­ate bis­[(2E)-but-2-enedioic acid]}, 2C(12)H(19)N(2)O(+)·C(4)H(2)O(4) (2−)·2C(4)H(4)O(4), has a single oxotremorine monocation protonated at the pyrrolidine nitro­gen, one fumaric acid mol­ecule and half of a fumarate dianion in the asymmetric unit. The ions and fumaric acid mol­ecules are held together by N—H⋯O and O–H-⋯O hydrogen bonds in 40-membered rings with graph-set notation R (6) (6)(40). The fumarate ions join these rings into infinite chains along [001]. [Image: see text] International Union of Crystallography 2022-04-07 /pmc/articles/PMC9462024/ /pubmed/36337690 http://dx.doi.org/10.1107/S2414314622003649 Text en © Naeem et al. 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Naeem, Marilyn
Chadeayne, Andrew R.
Golen, James A.
Manke, David R.
Bis(oxotremorine) fumarate bis­(fumaric acid)
title Bis(oxotremorine) fumarate bis­(fumaric acid)
title_full Bis(oxotremorine) fumarate bis­(fumaric acid)
title_fullStr Bis(oxotremorine) fumarate bis­(fumaric acid)
title_full_unstemmed Bis(oxotremorine) fumarate bis­(fumaric acid)
title_short Bis(oxotremorine) fumarate bis­(fumaric acid)
title_sort bis(oxotremorine) fumarate bis­(fumaric acid)
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462024/
https://www.ncbi.nlm.nih.gov/pubmed/36337690
http://dx.doi.org/10.1107/S2414314622003649
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AT mankedavidr bisoxotremorinefumaratebisfumaricacid

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