5-Methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1H-pyrazol-4-yl)-2-phenyl-1H-pyrazol-3(2H)-one

The title compound, C(20)H(18)N(4)O(2), known as bis­pyrazolone, was crystallized from dimethyl sulfoxide. The structure has ortho­rhom­bic (Pbca) symmetry at 150 K, and displays both intra- and inter­molecular hydrogen bonding through C—H⋯O and N—H⋯O contacts, respectively. None of the phenyl and p...

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Detalles Bibliográficos
Autores principales: Powell, Gregory L., Rix, Brad A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2020
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462187/
https://www.ncbi.nlm.nih.gov/pubmed/36340839
http://dx.doi.org/10.1107/S2414314620001212
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author Powell, Gregory L.
Rix, Brad A.
author_facet Powell, Gregory L.
Rix, Brad A.
author_sort Powell, Gregory L.
collection PubMed
description The title compound, C(20)H(18)N(4)O(2), known as bis­pyrazolone, was crystallized from dimethyl sulfoxide. The structure has ortho­rhom­bic (Pbca) symmetry at 150 K, and displays both intra- and inter­molecular hydrogen bonding through C—H⋯O and N—H⋯O contacts, respectively. None of the phenyl and pyrazolone rings in the mol­ecule are coplanar. The dihedral angle between the pyrazolone rings is 66.18 (5)°. [Image: see text]
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spelling pubmed-94621872022-11-04 5-Methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1H-pyrazol-4-yl)-2-phenyl-1H-pyrazol-3(2H)-one Powell, Gregory L. Rix, Brad A. IUCrdata Data Reports The title compound, C(20)H(18)N(4)O(2), known as bis­pyrazolone, was crystallized from dimethyl sulfoxide. The structure has ortho­rhom­bic (Pbca) symmetry at 150 K, and displays both intra- and inter­molecular hydrogen bonding through C—H⋯O and N—H⋯O contacts, respectively. None of the phenyl and pyrazolone rings in the mol­ecule are coplanar. The dihedral angle between the pyrazolone rings is 66.18 (5)°. [Image: see text] International Union of Crystallography 2020-02-11 /pmc/articles/PMC9462187/ /pubmed/36340839 http://dx.doi.org/10.1107/S2414314620001212 Text en © Powell and Rix 2020 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Powell, Gregory L.
Rix, Brad A.
5-Methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1H-pyrazol-4-yl)-2-phenyl-1H-pyrazol-3(2H)-one
title 5-Methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1H-pyrazol-4-yl)-2-phenyl-1H-pyrazol-3(2H)-one
title_full 5-Methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1H-pyrazol-4-yl)-2-phenyl-1H-pyrazol-3(2H)-one
title_fullStr 5-Methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1H-pyrazol-4-yl)-2-phenyl-1H-pyrazol-3(2H)-one
title_full_unstemmed 5-Methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1H-pyrazol-4-yl)-2-phenyl-1H-pyrazol-3(2H)-one
title_short 5-Methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1H-pyrazol-4-yl)-2-phenyl-1H-pyrazol-3(2H)-one
title_sort 5-methyl-4-(5-methyl-3-oxo-2-phenyl-2,3-di­hydro-1h-pyrazol-4-yl)-2-phenyl-1h-pyrazol-3(2h)-one
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462187/
https://www.ncbi.nlm.nih.gov/pubmed/36340839
http://dx.doi.org/10.1107/S2414314620001212
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