(S)-2-[(4-Fluoro­phen­yl)formamido]-3-phenyl­propanoic acid

The title compound, C(16)H(14)FNO(3), was synthesized via solid phase methods; it exhibits monoclinic (P2(1)) symmetry at room temperature. The two independent mol­ecules that comprise the asymmetric unit display distinct torsion angles of 173.2 (2) and 72.6 (2)° along the central sp (3) C—N bond. I...

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Detalles Bibliográficos
Autores principales: Lee, Kathleen S., Turner, Luke, Powell, Cynthia B., Reinheimer, Eric W.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2020
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462245/
https://www.ncbi.nlm.nih.gov/pubmed/36339782
http://dx.doi.org/10.1107/S2414314620008974
Descripción
Sumario:The title compound, C(16)H(14)FNO(3), was synthesized via solid phase methods; it exhibits monoclinic (P2(1)) symmetry at room temperature. The two independent mol­ecules that comprise the asymmetric unit display distinct torsion angles of 173.2 (2) and 72.6 (2)° along the central sp (3) C—N bond. In the crystal, hydrogen bonding through N—H⋯O contacts couples the asymmetric unit mol­ecules into pairs that align in layers extending parallel to (100) via additional O—H⋯O inter­actions. The phenyl ring of one independent mol­ecule was found to be disordered over two sets of sites in a 0.55 (3):0.45 (3) ratio. [Image: see text]

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