Diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate)

In the title compound, C(29)H(25)FN(2)O(4), the mean planes of the indole ring systems are approximately perpendicular to one another [dihedral angle = 88.3 (4)°]. The benzene ring is twisted with respect to the indole ring systems by 49.8 (5) and 77.6 (3)°. In the crystal, pairs of N—H⋯O hydrogen b...

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Autores principales: Jiang, Hong, Li, Yu-Long, Zhou, Jin, Sun, Hong-Shun, Zhang, Qing-Yu, Shi, Xing-Hao, Zhang, Zhi-Yuan, Ling, Tian
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2020
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462259/
https://www.ncbi.nlm.nih.gov/pubmed/36339780
http://dx.doi.org/10.1107/S2414314620009128
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author Jiang, Hong
Li, Yu-Long
Zhou, Jin
Sun, Hong-Shun
Zhang, Qing-Yu
Shi, Xing-Hao
Zhang, Zhi-Yuan
Ling, Tian
author_facet Jiang, Hong
Li, Yu-Long
Zhou, Jin
Sun, Hong-Shun
Zhang, Qing-Yu
Shi, Xing-Hao
Zhang, Zhi-Yuan
Ling, Tian
author_sort Jiang, Hong
collection PubMed
description In the title compound, C(29)H(25)FN(2)O(4), the mean planes of the indole ring systems are approximately perpendicular to one another [dihedral angle = 88.3 (4)°]. The benzene ring is twisted with respect to the indole ring systems by 49.8 (5) and 77.6 (3)°. In the crystal, pairs of N—H⋯O hydrogen bonds link the mol­ecules into the inversion dimers which are further linked into supra­molecular chains propagating along the [110] direction. [Image: see text]
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spelling pubmed-94622592022-11-04 Diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate) Jiang, Hong Li, Yu-Long Zhou, Jin Sun, Hong-Shun Zhang, Qing-Yu Shi, Xing-Hao Zhang, Zhi-Yuan Ling, Tian IUCrdata Data Reports In the title compound, C(29)H(25)FN(2)O(4), the mean planes of the indole ring systems are approximately perpendicular to one another [dihedral angle = 88.3 (4)°]. The benzene ring is twisted with respect to the indole ring systems by 49.8 (5) and 77.6 (3)°. In the crystal, pairs of N—H⋯O hydrogen bonds link the mol­ecules into the inversion dimers which are further linked into supra­molecular chains propagating along the [110] direction. [Image: see text] International Union of Crystallography 2020-07-10 /pmc/articles/PMC9462259/ /pubmed/36339780 http://dx.doi.org/10.1107/S2414314620009128 Text en © Jiang et al. 2020 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Jiang, Hong
Li, Yu-Long
Zhou, Jin
Sun, Hong-Shun
Zhang, Qing-Yu
Shi, Xing-Hao
Zhang, Zhi-Yuan
Ling, Tian
Diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate)
title Diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate)
title_full Diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate)
title_fullStr Diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate)
title_full_unstemmed Diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate)
title_short Diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate)
title_sort diethyl 3,3′-[(3-fluoro­phen­yl)methyl­ene]bis­(1h-indole-2-carboxyl­ate)
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462259/
https://www.ncbi.nlm.nih.gov/pubmed/36339780
http://dx.doi.org/10.1107/S2414314620009128
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