Dimethyl 3,3′-[(4-nitro­phen­yl)methyl­ene]bis­(1H-indole-2-carboxyl­ate) ethanol hemisolvate

There are two main molecules in asymmetric unit of the title compound, C(27)H(21)N(3)O(6)·0.5C(2)H(5)OH. In both, the indole ring systems are approximately perpendicular to each other, at dihedral angles of 69.3 (5) and 82.8(4)°. In the crystal, mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen bond...

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Detalles Bibliográficos
Autores principales: Li, Yu-Long, Zhou, Jin, Jiang, Hong, Sun, Hong-Shun, Li, Rui-Zhe, Liu, Sha-Li, Zhang, Xu-Dong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2021
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462316/
https://www.ncbi.nlm.nih.gov/pubmed/36338863
http://dx.doi.org/10.1107/S2414314621000572
Descripción
Sumario:There are two main molecules in asymmetric unit of the title compound, C(27)H(21)N(3)O(6)·0.5C(2)H(5)OH. In both, the indole ring systems are approximately perpendicular to each other, at dihedral angles of 69.3 (5) and 82.8(4)°. In the crystal, mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen bonds into a three-dimensional supra­molecular architecture. The solvent ethanol mol­ecule acts as a donor, forming an O—H⋯O hydrogen bond, reinforcing the structure. [Image: see text]

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