(3E)-4-[(Naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate

The title compound, C(15)H(15)NO·0.5H(2)O, was prepared from α-naphthyl­amine and 2,4-penta­nedione in a 1:1 ratio. An intra­molecular N—H⋯O hydrogen bond in the N-naphthyl­pent-3-en-2-one mol­ecule involving the amine and carbonyl groups strengthens the structure. The water mol­ecule interacts with...

Descripción completa

Detalles Bibliográficos
Autores principales: Diop, Aboubacar, Diop, Tidiane, Diop, Cheikh Abdou Khadre, Tumanov, Nikolay, Ennio, Zangrando, Sidibé, Mamadou
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2021
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462373/
https://www.ncbi.nlm.nih.gov/pubmed/36338948
http://dx.doi.org/10.1107/S2414314621009895
_version_ 1784787172969152512
author Diop, Aboubacar
Diop, Tidiane
Diop, Cheikh Abdou Khadre
Tumanov, Nikolay
Ennio, Zangrando
Sidibé, Mamadou
author_facet Diop, Aboubacar
Diop, Tidiane
Diop, Cheikh Abdou Khadre
Tumanov, Nikolay
Ennio, Zangrando
Sidibé, Mamadou
author_sort Diop, Aboubacar
collection PubMed
description The title compound, C(15)H(15)NO·0.5H(2)O, was prepared from α-naphthyl­amine and 2,4-penta­nedione in a 1:1 ratio. An intra­molecular N—H⋯O hydrogen bond in the N-naphthyl­pent-3-en-2-one mol­ecule involving the amine and carbonyl groups strengthens the structure. The water mol­ecule interacts with two symmetry-related N-naphthyl­pent-3-en-2-one mol­ecules viaby O—H⋯O hydrogen bonds. [Image: see text]
format Online
Article
Text
id pubmed-9462373
institution National Center for Biotechnology Information
language English
publishDate 2021
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-94623732022-11-04 (3E)-4-[(Naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate Diop, Aboubacar Diop, Tidiane Diop, Cheikh Abdou Khadre Tumanov, Nikolay Ennio, Zangrando Sidibé, Mamadou IUCrdata Data Reports The title compound, C(15)H(15)NO·0.5H(2)O, was prepared from α-naphthyl­amine and 2,4-penta­nedione in a 1:1 ratio. An intra­molecular N—H⋯O hydrogen bond in the N-naphthyl­pent-3-en-2-one mol­ecule involving the amine and carbonyl groups strengthens the structure. The water mol­ecule interacts with two symmetry-related N-naphthyl­pent-3-en-2-one mol­ecules viaby O—H⋯O hydrogen bonds. [Image: see text] International Union of Crystallography 2021-09-30 /pmc/articles/PMC9462373/ /pubmed/36338948 http://dx.doi.org/10.1107/S2414314621009895 Text en © Diop et al. 2021 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Diop, Aboubacar
Diop, Tidiane
Diop, Cheikh Abdou Khadre
Tumanov, Nikolay
Ennio, Zangrando
Sidibé, Mamadou
(3E)-4-[(Naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate
title (3E)-4-[(Naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate
title_full (3E)-4-[(Naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate
title_fullStr (3E)-4-[(Naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate
title_full_unstemmed (3E)-4-[(Naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate
title_short (3E)-4-[(Naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate
title_sort (3e)-4-[(naphthalen-1-yl)amino]­pent-3-en-2-one hemihydrate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462373/
https://www.ncbi.nlm.nih.gov/pubmed/36338948
http://dx.doi.org/10.1107/S2414314621009895
work_keys_str_mv AT diopaboubacar 3e4naphthalen1ylaminopent3en2onehemihydrate
AT dioptidiane 3e4naphthalen1ylaminopent3en2onehemihydrate
AT diopcheikhabdoukhadre 3e4naphthalen1ylaminopent3en2onehemihydrate
AT tumanovnikolay 3e4naphthalen1ylaminopent3en2onehemihydrate
AT enniozangrando 3e4naphthalen1ylaminopent3en2onehemihydrate
AT sidibemamadou 3e4naphthalen1ylaminopent3en2onehemihydrate

Ejemplares similares