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Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method

[Image: see text] SiO(2) ceramic parts with complex structures were formed by additive manufacturing technology via a light curing method combined with a heat treatment process. To reveal the influence mechanism of rheology and formability of SiO(2) ceramic slurry, the microstructure, morphology, an...

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Detalles Bibliográficos
Autores principales: Xu, Sanqiang, Fang, Man, Yan, Xiaokang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9476170/
https://www.ncbi.nlm.nih.gov/pubmed/36120074
http://dx.doi.org/10.1021/acsomega.2c04541
Descripción
Sumario:[Image: see text] SiO(2) ceramic parts with complex structures were formed by additive manufacturing technology via a light curing method combined with a heat treatment process. To reveal the influence mechanism of rheology and formability of SiO(2) ceramic slurry, the microstructure, morphology, and properties of light-cured SiO(2) ceramic samples were characterized by a viscosity test, thermogravimetric analysis (TG-DTG), X-ray diffraction (XRD), a scanning electron microscope (SEM), and a series of tests for physical properties (bending strength, mass burning rate, and densification). The results indicate that the main effect of the dispersant-type factor was more significant than the pH value. When the dispersant was ammonium polyacrylate (PMAA-NH(4)) with a content of 1.0 wt % and the pH value of the slurry system was 9, the viscosity of SiO(2) ceramic slurry could be controlled to the lowest. It was also found that the sintering temperature in the experiment had no effect on the crystalline phase of SiO(2) ceramics. When the sintering temperature was 1250 °C and the solid content was 65 vol %, the micromorphology of the samples was uniform. Under this condition, the bending strength of the sample reached 14.9 MPa and the densification was 76.43%.