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Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method

[Image: see text] SiO(2) ceramic parts with complex structures were formed by additive manufacturing technology via a light curing method combined with a heat treatment process. To reveal the influence mechanism of rheology and formability of SiO(2) ceramic slurry, the microstructure, morphology, an...

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Autores principales: Xu, Sanqiang, Fang, Man, Yan, Xiaokang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9476170/
https://www.ncbi.nlm.nih.gov/pubmed/36120074
http://dx.doi.org/10.1021/acsomega.2c04541
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author Xu, Sanqiang
Fang, Man
Yan, Xiaokang
author_facet Xu, Sanqiang
Fang, Man
Yan, Xiaokang
author_sort Xu, Sanqiang
collection PubMed
description [Image: see text] SiO(2) ceramic parts with complex structures were formed by additive manufacturing technology via a light curing method combined with a heat treatment process. To reveal the influence mechanism of rheology and formability of SiO(2) ceramic slurry, the microstructure, morphology, and properties of light-cured SiO(2) ceramic samples were characterized by a viscosity test, thermogravimetric analysis (TG-DTG), X-ray diffraction (XRD), a scanning electron microscope (SEM), and a series of tests for physical properties (bending strength, mass burning rate, and densification). The results indicate that the main effect of the dispersant-type factor was more significant than the pH value. When the dispersant was ammonium polyacrylate (PMAA-NH(4)) with a content of 1.0 wt % and the pH value of the slurry system was 9, the viscosity of SiO(2) ceramic slurry could be controlled to the lowest. It was also found that the sintering temperature in the experiment had no effect on the crystalline phase of SiO(2) ceramics. When the sintering temperature was 1250 °C and the solid content was 65 vol %, the micromorphology of the samples was uniform. Under this condition, the bending strength of the sample reached 14.9 MPa and the densification was 76.43%.
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spelling pubmed-94761702022-09-16 Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method Xu, Sanqiang Fang, Man Yan, Xiaokang ACS Omega [Image: see text] SiO(2) ceramic parts with complex structures were formed by additive manufacturing technology via a light curing method combined with a heat treatment process. To reveal the influence mechanism of rheology and formability of SiO(2) ceramic slurry, the microstructure, morphology, and properties of light-cured SiO(2) ceramic samples were characterized by a viscosity test, thermogravimetric analysis (TG-DTG), X-ray diffraction (XRD), a scanning electron microscope (SEM), and a series of tests for physical properties (bending strength, mass burning rate, and densification). The results indicate that the main effect of the dispersant-type factor was more significant than the pH value. When the dispersant was ammonium polyacrylate (PMAA-NH(4)) with a content of 1.0 wt % and the pH value of the slurry system was 9, the viscosity of SiO(2) ceramic slurry could be controlled to the lowest. It was also found that the sintering temperature in the experiment had no effect on the crystalline phase of SiO(2) ceramics. When the sintering temperature was 1250 °C and the solid content was 65 vol %, the micromorphology of the samples was uniform. Under this condition, the bending strength of the sample reached 14.9 MPa and the densification was 76.43%. American Chemical Society 2022-09-02 /pmc/articles/PMC9476170/ /pubmed/36120074 http://dx.doi.org/10.1021/acsomega.2c04541 Text en © 2022 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by-nc-nd/4.0/Permits non-commercial access and re-use, provided that author attribution and integrity are maintained; but does not permit creation of adaptations or other derivative works (https://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Xu, Sanqiang
Fang, Man
Yan, Xiaokang
Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method
title Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method
title_full Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method
title_fullStr Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method
title_full_unstemmed Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method
title_short Research on Rheology and Formability of SiO(2) Ceramic Slurry Based on Additive Manufacturing Technology via a Light Curing Method
title_sort research on rheology and formability of sio(2) ceramic slurry based on additive manufacturing technology via a light curing method
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9476170/
https://www.ncbi.nlm.nih.gov/pubmed/36120074
http://dx.doi.org/10.1021/acsomega.2c04541
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