A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy

Photochemical synthesis and photocatalysis in droplet microreactors represent promising approaches to relieve the global energy and environmental crises. Here, we describe a protocol for studying microdroplet photoreaction at an individual droplet level based on insitu micro-Raman spectroscopy. We p...

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Detalles Bibliográficos
Autores principales: Li, Kejian, Wang, Longqian, Liu, Juan, Gong, Kedong, Wang, Wei, Ge, Qiuyue, Liu, Yangyang, Zhang, Liwu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2022
Materias:
Protocol
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9494287/
https://www.ncbi.nlm.nih.gov/pubmed/36129823
http://dx.doi.org/10.1016/j.xpro.2022.101704
Descripción
Sumario:Photochemical synthesis and photocatalysis in droplet microreactors represent promising approaches to relieve the global energy and environmental crises. Here, we describe a protocol for studying microdroplet photoreaction at an individual droplet level based on insitu micro-Raman spectroscopy. We provide details of superhydrophobic substrate preparation, microdroplets generation, photoreactions performing, and data analyses. In addition, we show the operational details of preliminary scale-up tests of microdroplet photoreaction for practical application. For complete details on the use and execution of this protocol, please refer to Li et al. (2022).

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