A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy

Photochemical synthesis and photocatalysis in droplet microreactors represent promising approaches to relieve the global energy and environmental crises. Here, we describe a protocol for studying microdroplet photoreaction at an individual droplet level based on insitu micro-Raman spectroscopy. We p...

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Detalles Bibliográficos
Autores principales: Li, Kejian, Wang, Longqian, Liu, Juan, Gong, Kedong, Wang, Wei, Ge, Qiuyue, Liu, Yangyang, Zhang, Liwu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2022
Materias:
Protocol
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9494287/
https://www.ncbi.nlm.nih.gov/pubmed/36129823
http://dx.doi.org/10.1016/j.xpro.2022.101704
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author Li, Kejian
Wang, Longqian
Liu, Juan
Gong, Kedong
Wang, Wei
Ge, Qiuyue
Liu, Yangyang
Zhang, Liwu
author_facet Li, Kejian
Wang, Longqian
Liu, Juan
Gong, Kedong
Wang, Wei
Ge, Qiuyue
Liu, Yangyang
Zhang, Liwu
author_sort Li, Kejian
collection PubMed
description Photochemical synthesis and photocatalysis in droplet microreactors represent promising approaches to relieve the global energy and environmental crises. Here, we describe a protocol for studying microdroplet photoreaction at an individual droplet level based on insitu micro-Raman spectroscopy. We provide details of superhydrophobic substrate preparation, microdroplets generation, photoreactions performing, and data analyses. In addition, we show the operational details of preliminary scale-up tests of microdroplet photoreaction for practical application. For complete details on the use and execution of this protocol, please refer to Li et al. (2022).
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spelling pubmed-94942872022-09-23 A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy Li, Kejian Wang, Longqian Liu, Juan Gong, Kedong Wang, Wei Ge, Qiuyue Liu, Yangyang Zhang, Liwu STAR Protoc Protocol Photochemical synthesis and photocatalysis in droplet microreactors represent promising approaches to relieve the global energy and environmental crises. Here, we describe a protocol for studying microdroplet photoreaction at an individual droplet level based on insitu micro-Raman spectroscopy. We provide details of superhydrophobic substrate preparation, microdroplets generation, photoreactions performing, and data analyses. In addition, we show the operational details of preliminary scale-up tests of microdroplet photoreaction for practical application. For complete details on the use and execution of this protocol, please refer to Li et al. (2022). Elsevier 2022-09-20 /pmc/articles/PMC9494287/ /pubmed/36129823 http://dx.doi.org/10.1016/j.xpro.2022.101704 Text en © 2022 The Author(s) https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Protocol
Li, Kejian
Wang, Longqian
Liu, Juan
Gong, Kedong
Wang, Wei
Ge, Qiuyue
Liu, Yangyang
Zhang, Liwu
A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy
title A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy
title_full A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy
title_fullStr A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy
title_full_unstemmed A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy
title_short A protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-Raman spectroscopy
title_sort protocol to study microdroplet photoreaction at an individual droplet level using insitu micro-raman spectroscopy
topic Protocol
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9494287/
https://www.ncbi.nlm.nih.gov/pubmed/36129823
http://dx.doi.org/10.1016/j.xpro.2022.101704
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