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Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO(2)) Extraction

Patchouli extracts and oils extracted from Pogostemon cablin are essential raw material for the perfume and cosmetics industries, in addition to being used as a natural additive for food flavoring. Steam distillation is a standard method used for plant extraction. However, this method causes thermal...

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Autores principales: Muhammad, Syaifullah, H. P. S., Abdul Khalil, Abd Hamid, Shazlina, Danish, Mohammed, Marwan, M., Yunardi, Yunardi, Abdullah, C. K., Faisal, M., Yahya, Esam Bashir
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9503852/
https://www.ncbi.nlm.nih.gov/pubmed/36144760
http://dx.doi.org/10.3390/molecules27186025
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author Muhammad, Syaifullah
H. P. S., Abdul Khalil
Abd Hamid, Shazlina
Danish, Mohammed
Marwan, M.
Yunardi, Yunardi
Abdullah, C. K.
Faisal, M.
Yahya, Esam Bashir
author_facet Muhammad, Syaifullah
H. P. S., Abdul Khalil
Abd Hamid, Shazlina
Danish, Mohammed
Marwan, M.
Yunardi, Yunardi
Abdullah, C. K.
Faisal, M.
Yahya, Esam Bashir
author_sort Muhammad, Syaifullah
collection PubMed
description Patchouli extracts and oils extracted from Pogostemon cablin are essential raw material for the perfume and cosmetics industries, in addition to being used as a natural additive for food flavoring. Steam distillation is a standard method used for plant extraction. However, this method causes thermal degradation of some essential components of the oil. In this study, patchouli was extracted with supercritical carbon dioxide (SC-CO(2)) under different conditions of pressure (10–30 MPa) and temperature (40–80 °C). The chemical components of the crude extracted oil and the functional group were characterized using gas chromatography-mass spectrometry (GC-MS) and Fourier Transform Infrared Spectroscopy (FT-IR). The extraction with supercritical carbon dioxide was shown to provide a higher yield (12.41%) at a pressure of 20 MPa and a temperature of 80 °C. Patchouli alcohol, Azulene, δ-Guaiene, and Seychellene are the main bioactive compounds that GC-MS results have identified. FTIR spectra showed alcohol, aldehyde, and aromatic ring bond stretching peaks. Extraction of patchouli with supercritical carbon dioxide provided a higher yield and a better quality of the crude patchouli oil.
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spelling pubmed-95038522022-09-24 Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO(2)) Extraction Muhammad, Syaifullah H. P. S., Abdul Khalil Abd Hamid, Shazlina Danish, Mohammed Marwan, M. Yunardi, Yunardi Abdullah, C. K. Faisal, M. Yahya, Esam Bashir Molecules Article Patchouli extracts and oils extracted from Pogostemon cablin are essential raw material for the perfume and cosmetics industries, in addition to being used as a natural additive for food flavoring. Steam distillation is a standard method used for plant extraction. However, this method causes thermal degradation of some essential components of the oil. In this study, patchouli was extracted with supercritical carbon dioxide (SC-CO(2)) under different conditions of pressure (10–30 MPa) and temperature (40–80 °C). The chemical components of the crude extracted oil and the functional group were characterized using gas chromatography-mass spectrometry (GC-MS) and Fourier Transform Infrared Spectroscopy (FT-IR). The extraction with supercritical carbon dioxide was shown to provide a higher yield (12.41%) at a pressure of 20 MPa and a temperature of 80 °C. Patchouli alcohol, Azulene, δ-Guaiene, and Seychellene are the main bioactive compounds that GC-MS results have identified. FTIR spectra showed alcohol, aldehyde, and aromatic ring bond stretching peaks. Extraction of patchouli with supercritical carbon dioxide provided a higher yield and a better quality of the crude patchouli oil. MDPI 2022-09-15 /pmc/articles/PMC9503852/ /pubmed/36144760 http://dx.doi.org/10.3390/molecules27186025 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Muhammad, Syaifullah
H. P. S., Abdul Khalil
Abd Hamid, Shazlina
Danish, Mohammed
Marwan, M.
Yunardi, Yunardi
Abdullah, C. K.
Faisal, M.
Yahya, Esam Bashir
Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO(2)) Extraction
title Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO(2)) Extraction
title_full Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO(2)) Extraction
title_fullStr Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO(2)) Extraction
title_full_unstemmed Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO(2)) Extraction
title_short Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO(2)) Extraction
title_sort characterization of bioactive compounds from patchouli extracted via supercritical carbon dioxide (sc-co(2)) extraction
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9503852/
https://www.ncbi.nlm.nih.gov/pubmed/36144760
http://dx.doi.org/10.3390/molecules27186025
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