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Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes

Objective  Different post-sintering processes are expected to be a reason for alteration in the strength of zirconia. This study evaluated the effect of post-sintering processes on the flexural strength of different types of monolithic zirconia. Materials and Methods  A total of 120 classical- (Cz)...

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Autores principales: Juntavee, Niwut, Juntavee, Apa, Phattharasophachai, Thipradi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Thieme Medical and Scientific Publishers Pvt. Ltd. 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9507572/
https://www.ncbi.nlm.nih.gov/pubmed/35016234
http://dx.doi.org/10.1055/s-0041-1735937
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author Juntavee, Niwut
Juntavee, Apa
Phattharasophachai, Thipradi
author_facet Juntavee, Niwut
Juntavee, Apa
Phattharasophachai, Thipradi
author_sort Juntavee, Niwut
collection PubMed
description Objective  Different post-sintering processes are expected to be a reason for alteration in the strength of zirconia. This study evaluated the effect of post-sintering processes on the flexural strength of different types of monolithic zirconia. Materials and Methods  A total of 120 classical- (Cz) and high-translucent (Hz) monolithic zirconia discs (1.2 mm thickness and 14 mm in Ø) were prepared, sintered, and randomly divided into four groups to be surface-treated with (1) as-glazed (AG); (2) finished and polished (FP); (3) finished, polished, and overglazed (FPOG); and (4) finished, polished, and heat-treated (FPHT) technique ( n  = 15). Biaxial flexural strength (σ) was determined on a piston-on-three ball in a universal testing machine at a speed of 0.5 mm/min. Statistical Analysis  Analysis of variance, and post hoc Bonferroni multiple comparisons were determined for significant differences ( α = 0.05 ). Weibull analysis was applied for survival probability, Weibull modulus (m), and characteristic strength (σ (0) ). The microstructures were examined with a scanning electron microscope and X-ray diffraction. Results  The mean ± standard deviation value of σ (MPa), m, and σ (0) were 1,626.43 ± 184.38, 9.51, and 1,709.79 for CzAG; 1,734.98 ± 136.15, 12.83, and 1,799.17 for CzFP; 1,636.92 ± 130.11, 14.66, and 1,697.63 for CzFPOG; and 1,590.78 ± 161.74, 10.13, and 1,663.82 for CzFPHT; 643.30 ± 118.59, 5.59, and 695.55 for HzAG; 671.52 ± 96.77, 3.28, and 782.61 for HzFP; 556.33 ± 122.85, 4.76, and 607.01 for HzFPOG; and 598.36 ± 57.96, 11.22, and 624.89 for HzFPHT. The σ was significantly affected by the post-sintering process and type of zirconia ( p  < 0.05), but not by their interactions ( p  > 0.05). The Cz indicated a significantly higher σ than Hz. The FP process significantly enhanced σ more than other treatment procedures. Conclusion  Post-sintering processes enabled an alteration in σ of zirconia. FP enhanced σ, while FPOG and FPHT resulted in a reduction of σ. Glazing tends to induce defects at the glazing interface, while heat treatment induces a phase change to tetragonal, both resulted in reducing σ. Finishing and polishing for both Cz and Hz monolithic zirconia is recommended, while overglazed or heat-treated is not suggested.
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spelling pubmed-95075722022-09-24 Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes Juntavee, Niwut Juntavee, Apa Phattharasophachai, Thipradi Eur J Dent Objective  Different post-sintering processes are expected to be a reason for alteration in the strength of zirconia. This study evaluated the effect of post-sintering processes on the flexural strength of different types of monolithic zirconia. Materials and Methods  A total of 120 classical- (Cz) and high-translucent (Hz) monolithic zirconia discs (1.2 mm thickness and 14 mm in Ø) were prepared, sintered, and randomly divided into four groups to be surface-treated with (1) as-glazed (AG); (2) finished and polished (FP); (3) finished, polished, and overglazed (FPOG); and (4) finished, polished, and heat-treated (FPHT) technique ( n  = 15). Biaxial flexural strength (σ) was determined on a piston-on-three ball in a universal testing machine at a speed of 0.5 mm/min. Statistical Analysis  Analysis of variance, and post hoc Bonferroni multiple comparisons were determined for significant differences ( α = 0.05 ). Weibull analysis was applied for survival probability, Weibull modulus (m), and characteristic strength (σ (0) ). The microstructures were examined with a scanning electron microscope and X-ray diffraction. Results  The mean ± standard deviation value of σ (MPa), m, and σ (0) were 1,626.43 ± 184.38, 9.51, and 1,709.79 for CzAG; 1,734.98 ± 136.15, 12.83, and 1,799.17 for CzFP; 1,636.92 ± 130.11, 14.66, and 1,697.63 for CzFPOG; and 1,590.78 ± 161.74, 10.13, and 1,663.82 for CzFPHT; 643.30 ± 118.59, 5.59, and 695.55 for HzAG; 671.52 ± 96.77, 3.28, and 782.61 for HzFP; 556.33 ± 122.85, 4.76, and 607.01 for HzFPOG; and 598.36 ± 57.96, 11.22, and 624.89 for HzFPHT. The σ was significantly affected by the post-sintering process and type of zirconia ( p  < 0.05), but not by their interactions ( p  > 0.05). The Cz indicated a significantly higher σ than Hz. The FP process significantly enhanced σ more than other treatment procedures. Conclusion  Post-sintering processes enabled an alteration in σ of zirconia. FP enhanced σ, while FPOG and FPHT resulted in a reduction of σ. Glazing tends to induce defects at the glazing interface, while heat treatment induces a phase change to tetragonal, both resulted in reducing σ. Finishing and polishing for both Cz and Hz monolithic zirconia is recommended, while overglazed or heat-treated is not suggested. Thieme Medical and Scientific Publishers Pvt. Ltd. 2022-01-11 /pmc/articles/PMC9507572/ /pubmed/35016234 http://dx.doi.org/10.1055/s-0041-1735937 Text en The Author(s). This is an open access article published by Thieme under the terms of the Creative Commons Attribution License, permitting unrestricted use, distribution, and reproduction so long as the original work is properly cited. ( https://creativecommons.org/licenses/by/4.0/ ) https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Juntavee, Niwut
Juntavee, Apa
Phattharasophachai, Thipradi
Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes
title Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes
title_full Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes
title_fullStr Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes
title_full_unstemmed Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes
title_short Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes
title_sort biaxial flexural strength of different monolithic zirconia upon post-sintering processes
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9507572/
https://www.ncbi.nlm.nih.gov/pubmed/35016234
http://dx.doi.org/10.1055/s-0041-1735937
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