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Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber

Natural fiber-reinforced composite (NFRC) filaments for 3D printing were fabricated using polylactic acid (PLA) reinforced with 1–5 wt% henequen flour comprising particles with sizes between 90–250 μm. The flour was obtained from natural henequen fibers. NFRCs and pristine PLA specimens were printed...

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Autores principales: Agaliotis, Eliana M., Ake-Concha, Baltazar D., May-Pat, Alejandro, Morales-Arias, Juan P., Bernal, Celina, Valadez-Gonzalez, Alex, Herrera-Franco, Pedro J., Proust, Gwénaëlle, Koh-Dzul, J. Francisco, Carrillo, Jose G., Flores-Johnson, Emmanuel A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9570513/
https://www.ncbi.nlm.nih.gov/pubmed/36235924
http://dx.doi.org/10.3390/polym14193976
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author Agaliotis, Eliana M.
Ake-Concha, Baltazar D.
May-Pat, Alejandro
Morales-Arias, Juan P.
Bernal, Celina
Valadez-Gonzalez, Alex
Herrera-Franco, Pedro J.
Proust, Gwénaëlle
Koh-Dzul, J. Francisco
Carrillo, Jose G.
Flores-Johnson, Emmanuel A.
author_facet Agaliotis, Eliana M.
Ake-Concha, Baltazar D.
May-Pat, Alejandro
Morales-Arias, Juan P.
Bernal, Celina
Valadez-Gonzalez, Alex
Herrera-Franco, Pedro J.
Proust, Gwénaëlle
Koh-Dzul, J. Francisco
Carrillo, Jose G.
Flores-Johnson, Emmanuel A.
author_sort Agaliotis, Eliana M.
collection PubMed
description Natural fiber-reinforced composite (NFRC) filaments for 3D printing were fabricated using polylactic acid (PLA) reinforced with 1–5 wt% henequen flour comprising particles with sizes between 90–250 μm. The flour was obtained from natural henequen fibers. NFRCs and pristine PLA specimens were printed with a 0° raster angle for tension tests. The results showed that the NFRCs’ measured density, porosity, and degree of crystallinity increased with flour content. The tensile tests showed that the NFRC Young’s modulus was lower than that of the printed pristine PLA. For 1 wt% flour content, the NFRCs’ maximum stress and strain to failure were higher than those of the printed PLA, which was attributed to the henequen fibers acting as reinforcement and delaying crack growth. However, for 2 wt% and higher flour contents, the NFRCs’ maximum stress was lower than that of the printed PLA. Microscopic characterization after testing showed an increase in voids and defects, with the increase in flour content attributed to particle agglomeration. For 1 wt% flour content, the NFRCs were also printed with raster angles of ±45° and 90° for comparison; the highest tensile properties were obtained with a 0° raster angle. Finally, adding 3 wt% content of maleic anhydride to the NFRC with 1 wt% flour content slightly increased the maximum stress. The results presented herein warrant further research to fully understand the mechanical properties of printed NFRCs made of PLA reinforced with natural henequen fibers.
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spelling pubmed-95705132022-10-17 Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber Agaliotis, Eliana M. Ake-Concha, Baltazar D. May-Pat, Alejandro Morales-Arias, Juan P. Bernal, Celina Valadez-Gonzalez, Alex Herrera-Franco, Pedro J. Proust, Gwénaëlle Koh-Dzul, J. Francisco Carrillo, Jose G. Flores-Johnson, Emmanuel A. Polymers (Basel) Article Natural fiber-reinforced composite (NFRC) filaments for 3D printing were fabricated using polylactic acid (PLA) reinforced with 1–5 wt% henequen flour comprising particles with sizes between 90–250 μm. The flour was obtained from natural henequen fibers. NFRCs and pristine PLA specimens were printed with a 0° raster angle for tension tests. The results showed that the NFRCs’ measured density, porosity, and degree of crystallinity increased with flour content. The tensile tests showed that the NFRC Young’s modulus was lower than that of the printed pristine PLA. For 1 wt% flour content, the NFRCs’ maximum stress and strain to failure were higher than those of the printed PLA, which was attributed to the henequen fibers acting as reinforcement and delaying crack growth. However, for 2 wt% and higher flour contents, the NFRCs’ maximum stress was lower than that of the printed PLA. Microscopic characterization after testing showed an increase in voids and defects, with the increase in flour content attributed to particle agglomeration. For 1 wt% flour content, the NFRCs were also printed with raster angles of ±45° and 90° for comparison; the highest tensile properties were obtained with a 0° raster angle. Finally, adding 3 wt% content of maleic anhydride to the NFRC with 1 wt% flour content slightly increased the maximum stress. The results presented herein warrant further research to fully understand the mechanical properties of printed NFRCs made of PLA reinforced with natural henequen fibers. MDPI 2022-09-23 /pmc/articles/PMC9570513/ /pubmed/36235924 http://dx.doi.org/10.3390/polym14193976 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Agaliotis, Eliana M.
Ake-Concha, Baltazar D.
May-Pat, Alejandro
Morales-Arias, Juan P.
Bernal, Celina
Valadez-Gonzalez, Alex
Herrera-Franco, Pedro J.
Proust, Gwénaëlle
Koh-Dzul, J. Francisco
Carrillo, Jose G.
Flores-Johnson, Emmanuel A.
Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber
title Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber
title_full Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber
title_fullStr Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber
title_full_unstemmed Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber
title_short Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber
title_sort tensile behavior of 3d printed polylactic acid (pla) based composites reinforced with natural fiber
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9570513/
https://www.ncbi.nlm.nih.gov/pubmed/36235924
http://dx.doi.org/10.3390/polym14193976
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