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Cellulose Nanofibers from Schinus molle: Preparation and Characterization

Schinus molle (SM) was investigated as a primary source of cellulose with the aim of discovering resources to generate cellulose nanofibers (CNF). The SM was put through a soda pulping process to purify the cellulose, and then, the fiber was treated with an enzymatic treatment. Then, a twin-screw ex...

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Autores principales: Razzak, Abir, Khiari, Ramzi, Moussaoui, Younes, Belgacem, Mohamed Naceur
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9572333/
https://www.ncbi.nlm.nih.gov/pubmed/36235273
http://dx.doi.org/10.3390/molecules27196738
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author Razzak, Abir
Khiari, Ramzi
Moussaoui, Younes
Belgacem, Mohamed Naceur
author_facet Razzak, Abir
Khiari, Ramzi
Moussaoui, Younes
Belgacem, Mohamed Naceur
author_sort Razzak, Abir
collection PubMed
description Schinus molle (SM) was investigated as a primary source of cellulose with the aim of discovering resources to generate cellulose nanofibers (CNF). The SM was put through a soda pulping process to purify the cellulose, and then, the fiber was treated with an enzymatic treatment. Then, a twin-screw extruder and/or masuko were utilized to help with fiber delamination during the nanofibrillation process. After the enzymatic treatment, the twin-screw extruder and masuko treatment give a yield of 49.6 and 50.2%, respectively. The optical and atomic force microscopy, morfi, and polymerization degrees of prepared cellulosic materials were established. The pulp fibers, collected following each treatment stage, demonstrated that fiber characteristics such as length and crystallinity varied according to the used treatment (mechanical or enzymatic treatment). Obviously, the enzymic treatment resulted in shorter fibers and an increased degree of polymerization. However, the CNF obtained after enzymatic and extrusion treatment was achieved, and it gave 19 nm as the arithmetic width and a Young’s modulus of 8.63 GPa.
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spelling pubmed-95723332022-10-17 Cellulose Nanofibers from Schinus molle: Preparation and Characterization Razzak, Abir Khiari, Ramzi Moussaoui, Younes Belgacem, Mohamed Naceur Molecules Article Schinus molle (SM) was investigated as a primary source of cellulose with the aim of discovering resources to generate cellulose nanofibers (CNF). The SM was put through a soda pulping process to purify the cellulose, and then, the fiber was treated with an enzymatic treatment. Then, a twin-screw extruder and/or masuko were utilized to help with fiber delamination during the nanofibrillation process. After the enzymatic treatment, the twin-screw extruder and masuko treatment give a yield of 49.6 and 50.2%, respectively. The optical and atomic force microscopy, morfi, and polymerization degrees of prepared cellulosic materials were established. The pulp fibers, collected following each treatment stage, demonstrated that fiber characteristics such as length and crystallinity varied according to the used treatment (mechanical or enzymatic treatment). Obviously, the enzymic treatment resulted in shorter fibers and an increased degree of polymerization. However, the CNF obtained after enzymatic and extrusion treatment was achieved, and it gave 19 nm as the arithmetic width and a Young’s modulus of 8.63 GPa. MDPI 2022-10-09 /pmc/articles/PMC9572333/ /pubmed/36235273 http://dx.doi.org/10.3390/molecules27196738 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Razzak, Abir
Khiari, Ramzi
Moussaoui, Younes
Belgacem, Mohamed Naceur
Cellulose Nanofibers from Schinus molle: Preparation and Characterization
title Cellulose Nanofibers from Schinus molle: Preparation and Characterization
title_full Cellulose Nanofibers from Schinus molle: Preparation and Characterization
title_fullStr Cellulose Nanofibers from Schinus molle: Preparation and Characterization
title_full_unstemmed Cellulose Nanofibers from Schinus molle: Preparation and Characterization
title_short Cellulose Nanofibers from Schinus molle: Preparation and Characterization
title_sort cellulose nanofibers from schinus molle: preparation and characterization
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9572333/
https://www.ncbi.nlm.nih.gov/pubmed/36235273
http://dx.doi.org/10.3390/molecules27196738
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