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One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst
In the present research work, a novel catalyst based on natural material, namely, Fe(3)O(4)@nano-almondshell@OSi(CH(2))(3)/NHCH(2)pyridine/Cu(II) abbreviated (FNAOSiPAMP/Cu(II)) was designed and prepared. The properties of the catalyst was identified by Fourier-transform infrared spectroscopy (FT-IR...
Autores principales: | , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Nature Publishing Group UK
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9587238/ https://www.ncbi.nlm.nih.gov/pubmed/36271025 http://dx.doi.org/10.1038/s41598-022-22712-0 |
Sumario: | In the present research work, a novel catalyst based on natural material, namely, Fe(3)O(4)@nano-almondshell@OSi(CH(2))(3)/NHCH(2)pyridine/Cu(II) abbreviated (FNAOSiPAMP/Cu(II)) was designed and prepared. The properties of the catalyst was identified by Fourier-transform infrared spectroscopy (FT-IR), Thermogravimetry ananlysis (TG), X-ray diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDS), Field emission scanning electron microscopy (FESEM), Transmission electron microscopy (TEM), and Mapping. Furthermore, the evaluation of catalytic activity was done in the course of naphtho-1,3-oxazines synthesis. Solvent-free conditions, simplicity of operation, easy work-up and use of an eco-friendly catalyst are some of advantages of this protocol. |
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