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One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst

In the present research work, a novel catalyst based on natural material, namely, Fe(3)O(4)@nano-almondshell@OSi(CH(2))(3)/NHCH(2)pyridine/Cu(II) abbreviated (FNAOSiPAMP/Cu(II)) was designed and prepared. The properties of the catalyst was identified by Fourier-transform infrared spectroscopy (FT-IR...

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Detalles Bibliográficos
Autores principales: Keihanfar, Mina, Mirjalili, Bi Bi Fatemeh
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9587238/
https://www.ncbi.nlm.nih.gov/pubmed/36271025
http://dx.doi.org/10.1038/s41598-022-22712-0
Descripción
Sumario:In the present research work, a novel catalyst based on natural material, namely, Fe(3)O(4)@nano-almondshell@OSi(CH(2))(3)/NHCH(2)pyridine/Cu(II) abbreviated (FNAOSiPAMP/Cu(II)) was designed and prepared. The properties of the catalyst was identified by Fourier-transform infrared spectroscopy (FT-IR), Thermogravimetry ananlysis (TG), X-ray diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDS), Field emission scanning electron microscopy (FESEM), Transmission electron microscopy (TEM), and Mapping. Furthermore, the evaluation of catalytic activity was done in the course of naphtho-1,3-oxazines synthesis. Solvent-free conditions, simplicity of operation, easy work-up and use of an eco-friendly catalyst are some of advantages of this protocol.