One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst

In the present research work, a novel catalyst based on natural material, namely, Fe(3)O(4)@nano-almondshell@OSi(CH(2))(3)/NHCH(2)pyridine/Cu(II) abbreviated (FNAOSiPAMP/Cu(II)) was designed and prepared. The properties of the catalyst was identified by Fourier-transform infrared spectroscopy (FT-IR...

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Autores principales: Keihanfar, Mina, Mirjalili, Bi Bi Fatemeh
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9587238/
https://www.ncbi.nlm.nih.gov/pubmed/36271025
http://dx.doi.org/10.1038/s41598-022-22712-0
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author Keihanfar, Mina
Mirjalili, Bi Bi Fatemeh
author_facet Keihanfar, Mina
Mirjalili, Bi Bi Fatemeh
author_sort Keihanfar, Mina
collection PubMed
description In the present research work, a novel catalyst based on natural material, namely, Fe(3)O(4)@nano-almondshell@OSi(CH(2))(3)/NHCH(2)pyridine/Cu(II) abbreviated (FNAOSiPAMP/Cu(II)) was designed and prepared. The properties of the catalyst was identified by Fourier-transform infrared spectroscopy (FT-IR), Thermogravimetry ananlysis (TG), X-ray diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDS), Field emission scanning electron microscopy (FESEM), Transmission electron microscopy (TEM), and Mapping. Furthermore, the evaluation of catalytic activity was done in the course of naphtho-1,3-oxazines synthesis. Solvent-free conditions, simplicity of operation, easy work-up and use of an eco-friendly catalyst are some of advantages of this protocol.
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spelling pubmed-95872382022-10-23 One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst Keihanfar, Mina Mirjalili, Bi Bi Fatemeh Sci Rep Article In the present research work, a novel catalyst based on natural material, namely, Fe(3)O(4)@nano-almondshell@OSi(CH(2))(3)/NHCH(2)pyridine/Cu(II) abbreviated (FNAOSiPAMP/Cu(II)) was designed and prepared. The properties of the catalyst was identified by Fourier-transform infrared spectroscopy (FT-IR), Thermogravimetry ananlysis (TG), X-ray diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDS), Field emission scanning electron microscopy (FESEM), Transmission electron microscopy (TEM), and Mapping. Furthermore, the evaluation of catalytic activity was done in the course of naphtho-1,3-oxazines synthesis. Solvent-free conditions, simplicity of operation, easy work-up and use of an eco-friendly catalyst are some of advantages of this protocol. Nature Publishing Group UK 2022-10-21 /pmc/articles/PMC9587238/ /pubmed/36271025 http://dx.doi.org/10.1038/s41598-022-22712-0 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Keihanfar, Mina
Mirjalili, Bi Bi Fatemeh
One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst
title One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst
title_full One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst
title_fullStr One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst
title_full_unstemmed One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst
title_short One-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of FNAOSiPAMP*/Cu(II) as an almond shell based nanocatalyst
title_sort one-pot synthesis of naphtho[1,2-e][1,3]oxazines in the presence of fnaosipamp*/cu(ii) as an almond shell based nanocatalyst
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9587238/
https://www.ncbi.nlm.nih.gov/pubmed/36271025
http://dx.doi.org/10.1038/s41598-022-22712-0
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