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Effect of Wet Mixing on Properties of Radial-Orientation Basalt Fiber-Reinforced Rubber Compounds

The effects of wet mixing and traditional mixing on the properties of radial-orientation basalt fiber-reinforced rubber products were studied through experiments. The results show that compared with traditional mixing, the basalt fibers under the wet mixing conditions can more effectively enhance th...

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Autores principales: Yu, Benhui, Wang, Jing, Wang, Kongshuo, Han, Deshang, Ren, Jianbin, Zhang, Dewei, Wang, Chuansheng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9607495/
https://www.ncbi.nlm.nih.gov/pubmed/36298000
http://dx.doi.org/10.3390/polym14204422
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author Yu, Benhui
Wang, Jing
Wang, Kongshuo
Han, Deshang
Ren, Jianbin
Zhang, Dewei
Wang, Chuansheng
author_facet Yu, Benhui
Wang, Jing
Wang, Kongshuo
Han, Deshang
Ren, Jianbin
Zhang, Dewei
Wang, Chuansheng
author_sort Yu, Benhui
collection PubMed
description The effects of wet mixing and traditional mixing on the properties of radial-orientation basalt fiber-reinforced rubber products were studied through experiments. The results show that compared with traditional mixing, the basalt fibers under the wet mixing conditions can more effectively enhance the physical and mechanical properties of composites. The properties of the composites, such as carbon black dispersion, filler dispersion, rolling resistance and wet-sliding resistance, were the best after the latex and carbon black were premixed and then mixed by a mixer. Through extrusion experiments with the developed short-fiber radial-orientation die, it can be found that the fluidity of composites after extrusion is enhanced. Through analysis utilizing an electron microscope, it is shown that when the BFs added with KH550 (3-Aminopropyltriethoxysilane) were modified by KH560 ((3-Glycidyloxypropyl)trimethoxysilane), the interface layers of BF (basalt fiber)–KH560–NR and BF–KH550–NR were formed, which improves the adhesion between BFs and the rubber matrix. Qualitative characterization experiments on the orientation direction of the vulcanized composites were carried out through the experiments; that is, the qualitative characterization experiments on the segmented cutting and vulcanization of the composites in the radial direction showed that the short-fiber radial-orientation die could greatly improve the radial orientation degree of the short fibers in the radial direction. After adding KH560, the performance of the composites reinforced by the short fibers was improved to a certain extent compared with those without KH560. By adding DZ (N,N-Dicyclohexyl-2-benzothiazolsulfene amide) and CTP(cytidine triphosphate disodium) into the vulcanization system, the curing process of compounds in mixing and extrusion was delayed and the scorching resistance of short-fiber-reinforced composites was enhanced. Under the same conditions, the properties of the compounds after extrusion were greatly improved compared with those without extrusion.
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spelling pubmed-96074952022-10-28 Effect of Wet Mixing on Properties of Radial-Orientation Basalt Fiber-Reinforced Rubber Compounds Yu, Benhui Wang, Jing Wang, Kongshuo Han, Deshang Ren, Jianbin Zhang, Dewei Wang, Chuansheng Polymers (Basel) Article The effects of wet mixing and traditional mixing on the properties of radial-orientation basalt fiber-reinforced rubber products were studied through experiments. The results show that compared with traditional mixing, the basalt fibers under the wet mixing conditions can more effectively enhance the physical and mechanical properties of composites. The properties of the composites, such as carbon black dispersion, filler dispersion, rolling resistance and wet-sliding resistance, were the best after the latex and carbon black were premixed and then mixed by a mixer. Through extrusion experiments with the developed short-fiber radial-orientation die, it can be found that the fluidity of composites after extrusion is enhanced. Through analysis utilizing an electron microscope, it is shown that when the BFs added with KH550 (3-Aminopropyltriethoxysilane) were modified by KH560 ((3-Glycidyloxypropyl)trimethoxysilane), the interface layers of BF (basalt fiber)–KH560–NR and BF–KH550–NR were formed, which improves the adhesion between BFs and the rubber matrix. Qualitative characterization experiments on the orientation direction of the vulcanized composites were carried out through the experiments; that is, the qualitative characterization experiments on the segmented cutting and vulcanization of the composites in the radial direction showed that the short-fiber radial-orientation die could greatly improve the radial orientation degree of the short fibers in the radial direction. After adding KH560, the performance of the composites reinforced by the short fibers was improved to a certain extent compared with those without KH560. By adding DZ (N,N-Dicyclohexyl-2-benzothiazolsulfene amide) and CTP(cytidine triphosphate disodium) into the vulcanization system, the curing process of compounds in mixing and extrusion was delayed and the scorching resistance of short-fiber-reinforced composites was enhanced. Under the same conditions, the properties of the compounds after extrusion were greatly improved compared with those without extrusion. MDPI 2022-10-19 /pmc/articles/PMC9607495/ /pubmed/36298000 http://dx.doi.org/10.3390/polym14204422 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Yu, Benhui
Wang, Jing
Wang, Kongshuo
Han, Deshang
Ren, Jianbin
Zhang, Dewei
Wang, Chuansheng
Effect of Wet Mixing on Properties of Radial-Orientation Basalt Fiber-Reinforced Rubber Compounds
title Effect of Wet Mixing on Properties of Radial-Orientation Basalt Fiber-Reinforced Rubber Compounds
title_full Effect of Wet Mixing on Properties of Radial-Orientation Basalt Fiber-Reinforced Rubber Compounds
title_fullStr Effect of Wet Mixing on Properties of Radial-Orientation Basalt Fiber-Reinforced Rubber Compounds
title_full_unstemmed Effect of Wet Mixing on Properties of Radial-Orientation Basalt Fiber-Reinforced Rubber Compounds
title_short Effect of Wet Mixing on Properties of Radial-Orientation Basalt Fiber-Reinforced Rubber Compounds
title_sort effect of wet mixing on properties of radial-orientation basalt fiber-reinforced rubber compounds
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9607495/
https://www.ncbi.nlm.nih.gov/pubmed/36298000
http://dx.doi.org/10.3390/polym14204422
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