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Microstructure and Antibacterial Properties of Chitosan-Fe(3)O(4)-AgNP Nanocomposite
The goal of this research is to synthesize and characterize Fe(3)O(4)@Chitosan-AgNP nanocomposites in order to determine their antibacterial activity. The research methods include the synthesis of Fe(3)O(4)@Chitosan-AgNP nanocomposites, as well as the characterization of nanoparticles using scanning...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9610614/ https://www.ncbi.nlm.nih.gov/pubmed/36296842 http://dx.doi.org/10.3390/nano12203652 |
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author | Hartati, Hartati Subaer, Subaer Hasri, Hasri Wibawa, Teguh Hasriana, Hasriana |
author_facet | Hartati, Hartati Subaer, Subaer Hasri, Hasri Wibawa, Teguh Hasriana, Hasriana |
author_sort | Hartati, Hartati |
collection | PubMed |
description | The goal of this research is to synthesize and characterize Fe(3)O(4)@Chitosan-AgNP nanocomposites in order to determine their antibacterial activity. The research methods include the synthesis of Fe(3)O(4)@Chitosan-AgNP nanocomposites, as well as the characterization of nanoparticles using scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transform infrared (FTIR) analysis, and subsequent antibacterial activity tests. The study’s findings demonstrated the successful synthesis of Fe(3)O(4)@Chitosan-AgNP nanocomposites, followed by nanoparticle characterization using SEM, TEM, XRD, and FTIR. Based on the XRD results, the conjugation of Fe(3)O(4)@Chitosan-AgNP nanocomposites has been successfully formed, as evidenced by the appearance of characteristic peaks of Fe(3)O(4), chitosan, and AgNPs. According to the FTIR results, the interaction between chitosan-AgNPs and conjugated Fe(3)O(4) occurred via the N atom in the NH(2) group and the O atom in the OH group, and C=O. The SEM and TEM images also show that the Fe(3)O(4)@Chitosan-AgNP conjugation is a nanoparticle-based composite material. The combination of nanocomposites Fe(3)O(4)@Chitosan-AgNPs has antibacterial activity, inhibiting the growth of bacteria such as Bacillus cereus and Escherichia coli. |
format | Online Article Text |
id | pubmed-9610614 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-96106142022-10-28 Microstructure and Antibacterial Properties of Chitosan-Fe(3)O(4)-AgNP Nanocomposite Hartati, Hartati Subaer, Subaer Hasri, Hasri Wibawa, Teguh Hasriana, Hasriana Nanomaterials (Basel) Article The goal of this research is to synthesize and characterize Fe(3)O(4)@Chitosan-AgNP nanocomposites in order to determine their antibacterial activity. The research methods include the synthesis of Fe(3)O(4)@Chitosan-AgNP nanocomposites, as well as the characterization of nanoparticles using scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transform infrared (FTIR) analysis, and subsequent antibacterial activity tests. The study’s findings demonstrated the successful synthesis of Fe(3)O(4)@Chitosan-AgNP nanocomposites, followed by nanoparticle characterization using SEM, TEM, XRD, and FTIR. Based on the XRD results, the conjugation of Fe(3)O(4)@Chitosan-AgNP nanocomposites has been successfully formed, as evidenced by the appearance of characteristic peaks of Fe(3)O(4), chitosan, and AgNPs. According to the FTIR results, the interaction between chitosan-AgNPs and conjugated Fe(3)O(4) occurred via the N atom in the NH(2) group and the O atom in the OH group, and C=O. The SEM and TEM images also show that the Fe(3)O(4)@Chitosan-AgNP conjugation is a nanoparticle-based composite material. The combination of nanocomposites Fe(3)O(4)@Chitosan-AgNPs has antibacterial activity, inhibiting the growth of bacteria such as Bacillus cereus and Escherichia coli. MDPI 2022-10-18 /pmc/articles/PMC9610614/ /pubmed/36296842 http://dx.doi.org/10.3390/nano12203652 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Hartati, Hartati Subaer, Subaer Hasri, Hasri Wibawa, Teguh Hasriana, Hasriana Microstructure and Antibacterial Properties of Chitosan-Fe(3)O(4)-AgNP Nanocomposite |
title | Microstructure and Antibacterial Properties of Chitosan-Fe(3)O(4)-AgNP Nanocomposite |
title_full | Microstructure and Antibacterial Properties of Chitosan-Fe(3)O(4)-AgNP Nanocomposite |
title_fullStr | Microstructure and Antibacterial Properties of Chitosan-Fe(3)O(4)-AgNP Nanocomposite |
title_full_unstemmed | Microstructure and Antibacterial Properties of Chitosan-Fe(3)O(4)-AgNP Nanocomposite |
title_short | Microstructure and Antibacterial Properties of Chitosan-Fe(3)O(4)-AgNP Nanocomposite |
title_sort | microstructure and antibacterial properties of chitosan-fe(3)o(4)-agnp nanocomposite |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9610614/ https://www.ncbi.nlm.nih.gov/pubmed/36296842 http://dx.doi.org/10.3390/nano12203652 |
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