A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst

This manuscript reports an impressive and facile strategy for synthesizing isoxazole derivatives using immobilized Cu (I) in metformin-functionalized β-cyclodextrin as a catalyst. The architecture of this catalyst was characterized by different analytical techniques such as Fourier transform infrare...

Descripción completa

Detalles Bibliográficos
Autores principales: Tajbakhsh, Mahdieh, Naimi-Jamal, Mohammad Reza, Balalaie, Saeed, Rezaeian, Mohadeseh
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9646907/
https://www.ncbi.nlm.nih.gov/pubmed/36352247
http://dx.doi.org/10.1038/s41598-022-23814-5
_version_ 1784827268534632448
author Tajbakhsh, Mahdieh
Naimi-Jamal, Mohammad Reza
Balalaie, Saeed
Rezaeian, Mohadeseh
author_facet Tajbakhsh, Mahdieh
Naimi-Jamal, Mohammad Reza
Balalaie, Saeed
Rezaeian, Mohadeseh
author_sort Tajbakhsh, Mahdieh
collection PubMed
description This manuscript reports an impressive and facile strategy for synthesizing isoxazole derivatives using immobilized Cu (I) in metformin-functionalized β-cyclodextrin as a catalyst. The architecture of this catalyst was characterized by different analytical techniques such as Fourier transform infrared spectroscopy, Thermogravimetric analysis, X-ray diffraction, Field emission scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. The catalyst showed remarkable reusability even after 7 consecutive runs.
format Online
Article
Text
id pubmed-9646907
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher Nature Publishing Group UK
record_format MEDLINE/PubMed
spelling pubmed-96469072022-11-15 A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst Tajbakhsh, Mahdieh Naimi-Jamal, Mohammad Reza Balalaie, Saeed Rezaeian, Mohadeseh Sci Rep Article This manuscript reports an impressive and facile strategy for synthesizing isoxazole derivatives using immobilized Cu (I) in metformin-functionalized β-cyclodextrin as a catalyst. The architecture of this catalyst was characterized by different analytical techniques such as Fourier transform infrared spectroscopy, Thermogravimetric analysis, X-ray diffraction, Field emission scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. The catalyst showed remarkable reusability even after 7 consecutive runs. Nature Publishing Group UK 2022-11-09 /pmc/articles/PMC9646907/ /pubmed/36352247 http://dx.doi.org/10.1038/s41598-022-23814-5 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Tajbakhsh, Mahdieh
Naimi-Jamal, Mohammad Reza
Balalaie, Saeed
Rezaeian, Mohadeseh
A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst
title A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst
title_full A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst
title_fullStr A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst
title_full_unstemmed A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst
title_short A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst
title_sort green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4h)-ones using modified β-cyclodextrin as a catalyst
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9646907/
https://www.ncbi.nlm.nih.gov/pubmed/36352247
http://dx.doi.org/10.1038/s41598-022-23814-5
work_keys_str_mv AT tajbakhshmahdieh agreenprotocolfortheonepotsynthesisof34disubstitutedisoxazole54honesusingmodifiedbcyclodextrinasacatalyst
AT naimijamalmohammadreza agreenprotocolfortheonepotsynthesisof34disubstitutedisoxazole54honesusingmodifiedbcyclodextrinasacatalyst
AT balalaiesaeed agreenprotocolfortheonepotsynthesisof34disubstitutedisoxazole54honesusingmodifiedbcyclodextrinasacatalyst
AT rezaeianmohadeseh agreenprotocolfortheonepotsynthesisof34disubstitutedisoxazole54honesusingmodifiedbcyclodextrinasacatalyst
AT tajbakhshmahdieh greenprotocolfortheonepotsynthesisof34disubstitutedisoxazole54honesusingmodifiedbcyclodextrinasacatalyst
AT naimijamalmohammadreza greenprotocolfortheonepotsynthesisof34disubstitutedisoxazole54honesusingmodifiedbcyclodextrinasacatalyst
AT balalaiesaeed greenprotocolfortheonepotsynthesisof34disubstitutedisoxazole54honesusingmodifiedbcyclodextrinasacatalyst
AT rezaeianmohadeseh greenprotocolfortheonepotsynthesisof34disubstitutedisoxazole54honesusingmodifiedbcyclodextrinasacatalyst

Ejemplares similares