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Fabrication of Europium-Doped Barium Titanate/Polystyrene Polymer Nanocomposites Using Ultrasonication-Assisted Method: Structural and Optical Properties

In the current work, europium-doped barium titanate particles were used as filler material and polystyrene was used as a matrix to fabricate Ba(1−3x)/2Eu(x)TiO(3)/PS polymer nanocomposites with x = 0, 0.005, 0.015 and 0.025. A solid-state reaction was used to synthesize filler particles and the solv...

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Autores principales: Kumar, Umesh, Padalia, Diwakar, Bhandari, Prabhakar, Kumar, Pawan, Ranakoti, Lalit, Singh, Tej, Lendvai, László
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9655646/
https://www.ncbi.nlm.nih.gov/pubmed/36365657
http://dx.doi.org/10.3390/polym14214664
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author Kumar, Umesh
Padalia, Diwakar
Bhandari, Prabhakar
Kumar, Pawan
Ranakoti, Lalit
Singh, Tej
Lendvai, László
author_facet Kumar, Umesh
Padalia, Diwakar
Bhandari, Prabhakar
Kumar, Pawan
Ranakoti, Lalit
Singh, Tej
Lendvai, László
author_sort Kumar, Umesh
collection PubMed
description In the current work, europium-doped barium titanate particles were used as filler material and polystyrene was used as a matrix to fabricate Ba(1−3x)/2Eu(x)TiO(3)/PS polymer nanocomposites with x = 0, 0.005, 0.015 and 0.025. A solid-state reaction was used to synthesize filler particles and the solvent evaporation method was used to form polymer nanocomposites. The effects of ultrasonic treatment were also studied in the formation of nanocomposite materials. The quantitative and qualitative studies were conducted using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), and ultraviolet-visible (UV-Vis) characterization techniques. The XRD data and FTIR data confirm the incorporation of filler particles in the polymer matrix. FE-SEM data confirms that the particles are in the nanophase. The optical band gap was directly affected by the filler particles and it started to reduce as Eu concentration started to increase.
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spelling pubmed-96556462022-11-15 Fabrication of Europium-Doped Barium Titanate/Polystyrene Polymer Nanocomposites Using Ultrasonication-Assisted Method: Structural and Optical Properties Kumar, Umesh Padalia, Diwakar Bhandari, Prabhakar Kumar, Pawan Ranakoti, Lalit Singh, Tej Lendvai, László Polymers (Basel) Article In the current work, europium-doped barium titanate particles were used as filler material and polystyrene was used as a matrix to fabricate Ba(1−3x)/2Eu(x)TiO(3)/PS polymer nanocomposites with x = 0, 0.005, 0.015 and 0.025. A solid-state reaction was used to synthesize filler particles and the solvent evaporation method was used to form polymer nanocomposites. The effects of ultrasonic treatment were also studied in the formation of nanocomposite materials. The quantitative and qualitative studies were conducted using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), and ultraviolet-visible (UV-Vis) characterization techniques. The XRD data and FTIR data confirm the incorporation of filler particles in the polymer matrix. FE-SEM data confirms that the particles are in the nanophase. The optical band gap was directly affected by the filler particles and it started to reduce as Eu concentration started to increase. MDPI 2022-11-01 /pmc/articles/PMC9655646/ /pubmed/36365657 http://dx.doi.org/10.3390/polym14214664 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kumar, Umesh
Padalia, Diwakar
Bhandari, Prabhakar
Kumar, Pawan
Ranakoti, Lalit
Singh, Tej
Lendvai, László
Fabrication of Europium-Doped Barium Titanate/Polystyrene Polymer Nanocomposites Using Ultrasonication-Assisted Method: Structural and Optical Properties
title Fabrication of Europium-Doped Barium Titanate/Polystyrene Polymer Nanocomposites Using Ultrasonication-Assisted Method: Structural and Optical Properties
title_full Fabrication of Europium-Doped Barium Titanate/Polystyrene Polymer Nanocomposites Using Ultrasonication-Assisted Method: Structural and Optical Properties
title_fullStr Fabrication of Europium-Doped Barium Titanate/Polystyrene Polymer Nanocomposites Using Ultrasonication-Assisted Method: Structural and Optical Properties
title_full_unstemmed Fabrication of Europium-Doped Barium Titanate/Polystyrene Polymer Nanocomposites Using Ultrasonication-Assisted Method: Structural and Optical Properties
title_short Fabrication of Europium-Doped Barium Titanate/Polystyrene Polymer Nanocomposites Using Ultrasonication-Assisted Method: Structural and Optical Properties
title_sort fabrication of europium-doped barium titanate/polystyrene polymer nanocomposites using ultrasonication-assisted method: structural and optical properties
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9655646/
https://www.ncbi.nlm.nih.gov/pubmed/36365657
http://dx.doi.org/10.3390/polym14214664
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