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Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry
Solid-state NMR is a nondestructive and noninvasive technique used to study the chemical structure and dynamics of starch-based materials and to bridge the gap between structure–function relationships and industrial applications. The study of crystallinity, chemical modification, product blending, m...
Autores principales: | , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9657013/ https://www.ncbi.nlm.nih.gov/pubmed/36365679 http://dx.doi.org/10.3390/polym14214686 |
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author | El Nokab, Mustapha El Hariri Alassmy, Yasser A. Abduljawad, Marwan M. Al-shamrani, Khalid M. Alnafisah, Mohammed S. Asgar Pour, Zahra Tucker, Chelsea L. Sebakhy, Khaled O. |
author_facet | El Nokab, Mustapha El Hariri Alassmy, Yasser A. Abduljawad, Marwan M. Al-shamrani, Khalid M. Alnafisah, Mohammed S. Asgar Pour, Zahra Tucker, Chelsea L. Sebakhy, Khaled O. |
author_sort | El Nokab, Mustapha El Hariri |
collection | PubMed |
description | Solid-state NMR is a nondestructive and noninvasive technique used to study the chemical structure and dynamics of starch-based materials and to bridge the gap between structure–function relationships and industrial applications. The study of crystallinity, chemical modification, product blending, molecular packing, amylose–amylopectin ratio, end chain motion, and solvent–matrix interactions is essential for tailoring starch product properties to various applications. This article aims to provide a comprehensive and critical review of research characterizing starch-based materials using solid-state NMR, and to briefly introduce the most advanced and promising NMR strategies and hardware designs used to overcome the sensitivity and resolution issues involved in structure–function relationships. |
format | Online Article Text |
id | pubmed-9657013 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-96570132022-11-15 Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry El Nokab, Mustapha El Hariri Alassmy, Yasser A. Abduljawad, Marwan M. Al-shamrani, Khalid M. Alnafisah, Mohammed S. Asgar Pour, Zahra Tucker, Chelsea L. Sebakhy, Khaled O. Polymers (Basel) Review Solid-state NMR is a nondestructive and noninvasive technique used to study the chemical structure and dynamics of starch-based materials and to bridge the gap between structure–function relationships and industrial applications. The study of crystallinity, chemical modification, product blending, molecular packing, amylose–amylopectin ratio, end chain motion, and solvent–matrix interactions is essential for tailoring starch product properties to various applications. This article aims to provide a comprehensive and critical review of research characterizing starch-based materials using solid-state NMR, and to briefly introduce the most advanced and promising NMR strategies and hardware designs used to overcome the sensitivity and resolution issues involved in structure–function relationships. MDPI 2022-11-02 /pmc/articles/PMC9657013/ /pubmed/36365679 http://dx.doi.org/10.3390/polym14214686 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Review El Nokab, Mustapha El Hariri Alassmy, Yasser A. Abduljawad, Marwan M. Al-shamrani, Khalid M. Alnafisah, Mohammed S. Asgar Pour, Zahra Tucker, Chelsea L. Sebakhy, Khaled O. Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry |
title | Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry |
title_full | Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry |
title_fullStr | Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry |
title_full_unstemmed | Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry |
title_short | Solid-State NMR Spectroscopy: Towards Structural Insights into Starch-Based Materials in the Food Industry |
title_sort | solid-state nmr spectroscopy: towards structural insights into starch-based materials in the food industry |
topic | Review |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9657013/ https://www.ncbi.nlm.nih.gov/pubmed/36365679 http://dx.doi.org/10.3390/polym14214686 |
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