Cargando…

Influence of Extrusion Temperature on Properties of Graphene Oxide-Carbon Fiber/Epoxy Composite Prepared by Vacuum Infiltration Hot-Press-Forming Experimental System

Graphene oxide-carbon fiber/epoxy (GO-CF/EP) composites with extrusion temperatures of 30, 40, 50, 60 and 70 °C were prepared by a vacuum infiltration hot-press-forming experimental system (VIHPS). The effects of extrusion temperature on the microstructure, fracture mechanism and mechanical properti...

Descripción completa

Detalles Bibliográficos
Autores principales: Ma, Yuqin, Li, Fei, Xu, Wei, Zhang, Yuyang, Xu, Yi, Guo, Haiyin, Li, Yatao
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9657986/
https://www.ncbi.nlm.nih.gov/pubmed/36364615
http://dx.doi.org/10.3390/nano12213839
_version_ 1784829838841872384
author Ma, Yuqin
Li, Fei
Xu, Wei
Zhang, Yuyang
Xu, Yi
Guo, Haiyin
Li, Yatao
author_facet Ma, Yuqin
Li, Fei
Xu, Wei
Zhang, Yuyang
Xu, Yi
Guo, Haiyin
Li, Yatao
author_sort Ma, Yuqin
collection PubMed
description Graphene oxide-carbon fiber/epoxy (GO-CF/EP) composites with extrusion temperatures of 30, 40, 50, 60 and 70 °C were prepared by a vacuum infiltration hot-press-forming experimental system (VIHPS). The effects of extrusion temperature on the microstructure, fracture mechanism and mechanical properties of GO-CF/EP composites were investigated. It was found that the best mechanical property of composites and infiltration effect of the matrix in the fiber gap were obtained at the temperature of 50 °C, and the bending strength of the composite reached 728 MPa. The fiber was pulled out and broken under the wrapping of the matrix. The matrix viscosity was high, and the fluidity was poor when the extrusion temperature was low. The poor infiltration of the matrix resulted in many fibers failing to bond together, resulting in the disorderly breakage of fiber bundles. Under the condition of higher temperature, the flow speed of the matrix could be improved. However, part of the matrix was extruded during the extrusion process, and cracks and other defects occurred during the loading, which caused the brittle fracture of the specimen.
format Online
Article
Text
id pubmed-9657986
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-96579862022-11-15 Influence of Extrusion Temperature on Properties of Graphene Oxide-Carbon Fiber/Epoxy Composite Prepared by Vacuum Infiltration Hot-Press-Forming Experimental System Ma, Yuqin Li, Fei Xu, Wei Zhang, Yuyang Xu, Yi Guo, Haiyin Li, Yatao Nanomaterials (Basel) Article Graphene oxide-carbon fiber/epoxy (GO-CF/EP) composites with extrusion temperatures of 30, 40, 50, 60 and 70 °C were prepared by a vacuum infiltration hot-press-forming experimental system (VIHPS). The effects of extrusion temperature on the microstructure, fracture mechanism and mechanical properties of GO-CF/EP composites were investigated. It was found that the best mechanical property of composites and infiltration effect of the matrix in the fiber gap were obtained at the temperature of 50 °C, and the bending strength of the composite reached 728 MPa. The fiber was pulled out and broken under the wrapping of the matrix. The matrix viscosity was high, and the fluidity was poor when the extrusion temperature was low. The poor infiltration of the matrix resulted in many fibers failing to bond together, resulting in the disorderly breakage of fiber bundles. Under the condition of higher temperature, the flow speed of the matrix could be improved. However, part of the matrix was extruded during the extrusion process, and cracks and other defects occurred during the loading, which caused the brittle fracture of the specimen. MDPI 2022-10-30 /pmc/articles/PMC9657986/ /pubmed/36364615 http://dx.doi.org/10.3390/nano12213839 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ma, Yuqin
Li, Fei
Xu, Wei
Zhang, Yuyang
Xu, Yi
Guo, Haiyin
Li, Yatao
Influence of Extrusion Temperature on Properties of Graphene Oxide-Carbon Fiber/Epoxy Composite Prepared by Vacuum Infiltration Hot-Press-Forming Experimental System
title Influence of Extrusion Temperature on Properties of Graphene Oxide-Carbon Fiber/Epoxy Composite Prepared by Vacuum Infiltration Hot-Press-Forming Experimental System
title_full Influence of Extrusion Temperature on Properties of Graphene Oxide-Carbon Fiber/Epoxy Composite Prepared by Vacuum Infiltration Hot-Press-Forming Experimental System
title_fullStr Influence of Extrusion Temperature on Properties of Graphene Oxide-Carbon Fiber/Epoxy Composite Prepared by Vacuum Infiltration Hot-Press-Forming Experimental System
title_full_unstemmed Influence of Extrusion Temperature on Properties of Graphene Oxide-Carbon Fiber/Epoxy Composite Prepared by Vacuum Infiltration Hot-Press-Forming Experimental System
title_short Influence of Extrusion Temperature on Properties of Graphene Oxide-Carbon Fiber/Epoxy Composite Prepared by Vacuum Infiltration Hot-Press-Forming Experimental System
title_sort influence of extrusion temperature on properties of graphene oxide-carbon fiber/epoxy composite prepared by vacuum infiltration hot-press-forming experimental system
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9657986/
https://www.ncbi.nlm.nih.gov/pubmed/36364615
http://dx.doi.org/10.3390/nano12213839
work_keys_str_mv AT mayuqin influenceofextrusiontemperatureonpropertiesofgrapheneoxidecarbonfiberepoxycompositepreparedbyvacuuminfiltrationhotpressformingexperimentalsystem
AT lifei influenceofextrusiontemperatureonpropertiesofgrapheneoxidecarbonfiberepoxycompositepreparedbyvacuuminfiltrationhotpressformingexperimentalsystem
AT xuwei influenceofextrusiontemperatureonpropertiesofgrapheneoxidecarbonfiberepoxycompositepreparedbyvacuuminfiltrationhotpressformingexperimentalsystem
AT zhangyuyang influenceofextrusiontemperatureonpropertiesofgrapheneoxidecarbonfiberepoxycompositepreparedbyvacuuminfiltrationhotpressformingexperimentalsystem
AT xuyi influenceofextrusiontemperatureonpropertiesofgrapheneoxidecarbonfiberepoxycompositepreparedbyvacuuminfiltrationhotpressformingexperimentalsystem
AT guohaiyin influenceofextrusiontemperatureonpropertiesofgrapheneoxidecarbonfiberepoxycompositepreparedbyvacuuminfiltrationhotpressformingexperimentalsystem
AT liyatao influenceofextrusiontemperatureonpropertiesofgrapheneoxidecarbonfiberepoxycompositepreparedbyvacuuminfiltrationhotpressformingexperimentalsystem