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Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression

The formability of magnesium alloys can be significantly improved by Ca as an alloying addition. Compared to conventional alloy sheets such as AZ31, texture modification can be found in rolled Mg-Ca sheets, which reveal a randomized orientation distribution. The hot deformation behavior of a twin-ro...

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Autores principales: Kittner, Kristina, Ullmann, Madlen, Prahl, Ulrich
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9658210/
https://www.ncbi.nlm.nih.gov/pubmed/36363090
http://dx.doi.org/10.3390/ma15217499
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author Kittner, Kristina
Ullmann, Madlen
Prahl, Ulrich
author_facet Kittner, Kristina
Ullmann, Madlen
Prahl, Ulrich
author_sort Kittner, Kristina
collection PubMed
description The formability of magnesium alloys can be significantly improved by Ca as an alloying addition. Compared to conventional alloy sheets such as AZ31, texture modification can be found in rolled Mg-Ca sheets, which reveal a randomized orientation distribution. The hot deformation behavior of a twin-roll cast and homogenized Mg-2Zn-1Al-0.3Ca (ZAX210) alloy was characterized during hot compression at a temperature of 350 °C and strain rates of 0.1 s(−1) and 10 s(−1). Electron backscatter diffraction (EBSD) analysis was performed in order to describe the microstructural and texture evolution. The ZAX210 alloy exhibits a pronounced dynamic recrystallization (DRX) behavior during compression at high strain rates, while at lower strain rates DRX hardly occurred. This effect can be attributed to different DRX mechanisms that take place as a function of strain rate. At low strain rates, DRX occurred locally at the grain boundaries of the original microstructure, forming a so-called necklace structure. Increasing strain rate results in an increased fraction of recrystallized grains from 18% (0.1 s(−1)) to 39% (10 s(−1)). The microstructure revealed that twin boundaries act as nucleation sites for the DRX (TDRX). The recrystallized areas exhibit a weaker texture compared to the deformed microstructure.
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spelling pubmed-96582102022-11-15 Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression Kittner, Kristina Ullmann, Madlen Prahl, Ulrich Materials (Basel) Article The formability of magnesium alloys can be significantly improved by Ca as an alloying addition. Compared to conventional alloy sheets such as AZ31, texture modification can be found in rolled Mg-Ca sheets, which reveal a randomized orientation distribution. The hot deformation behavior of a twin-roll cast and homogenized Mg-2Zn-1Al-0.3Ca (ZAX210) alloy was characterized during hot compression at a temperature of 350 °C and strain rates of 0.1 s(−1) and 10 s(−1). Electron backscatter diffraction (EBSD) analysis was performed in order to describe the microstructural and texture evolution. The ZAX210 alloy exhibits a pronounced dynamic recrystallization (DRX) behavior during compression at high strain rates, while at lower strain rates DRX hardly occurred. This effect can be attributed to different DRX mechanisms that take place as a function of strain rate. At low strain rates, DRX occurred locally at the grain boundaries of the original microstructure, forming a so-called necklace structure. Increasing strain rate results in an increased fraction of recrystallized grains from 18% (0.1 s(−1)) to 39% (10 s(−1)). The microstructure revealed that twin boundaries act as nucleation sites for the DRX (TDRX). The recrystallized areas exhibit a weaker texture compared to the deformed microstructure. MDPI 2022-10-26 /pmc/articles/PMC9658210/ /pubmed/36363090 http://dx.doi.org/10.3390/ma15217499 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kittner, Kristina
Ullmann, Madlen
Prahl, Ulrich
Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression
title Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression
title_full Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression
title_fullStr Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression
title_full_unstemmed Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression
title_short Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression
title_sort microstructural and textural investigation of an mg-zn-al-ca alloy after hot plane strain compression
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9658210/
https://www.ncbi.nlm.nih.gov/pubmed/36363090
http://dx.doi.org/10.3390/ma15217499
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