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Self-extracted corn-stalk cellulose/epoxy resin composites
In order to make full use of crop waste stalk, corn-stalk cellulose (CSC) was extracted by acid–base method and used as modifier of epoxy resin (E51) to prepare the self-extracted corn-stalk cellulose/epoxy resin composites (CSCEC). Differential scanning calorimeter (DSC), thermogravimetry (TG) anal...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Nature Publishing Group UK
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9722901/ https://www.ncbi.nlm.nih.gov/pubmed/36471157 http://dx.doi.org/10.1038/s41598-022-25695-0 |
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author | Lou, Chunhua Jiang, Siyu Yan, An Zhou, Yongli Liu, Yang Zhang, Yong Kong, Xianzhi |
author_facet | Lou, Chunhua Jiang, Siyu Yan, An Zhou, Yongli Liu, Yang Zhang, Yong Kong, Xianzhi |
author_sort | Lou, Chunhua |
collection | PubMed |
description | In order to make full use of crop waste stalk, corn-stalk cellulose (CSC) was extracted by acid–base method and used as modifier of epoxy resin (E51) to prepare the self-extracted corn-stalk cellulose/epoxy resin composites (CSCEC). Differential scanning calorimeter (DSC), thermogravimetry (TG) analysis, dynamic mechanical analysis (DMA), morphology analysis by scanning electron microscope (SEM), the mechanical properties by electronic universal testing machine and impact testing machine were used for characterization and analysis. The experimental results showed that when the CSC content was 20 wt%, the impact strength of the composite was 2.50 kJ/m(2), which was 127.2% higher than that of pure epoxy resin. When the CSC content was 20 wt%, the Tg of epoxy resin obtained by DMA was the lowest, 167.4 °C, which decreased by 11.3 °C compared with that of pure epoxy resin. The SEM result showed that the fracture surface of the composite became obviously rough and had of obvious folds, which was a ductile fracture. These results indicated that the addition of CSC could toughen the epoxy resin. |
format | Online Article Text |
id | pubmed-9722901 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | Nature Publishing Group UK |
record_format | MEDLINE/PubMed |
spelling | pubmed-97229012022-12-07 Self-extracted corn-stalk cellulose/epoxy resin composites Lou, Chunhua Jiang, Siyu Yan, An Zhou, Yongli Liu, Yang Zhang, Yong Kong, Xianzhi Sci Rep Article In order to make full use of crop waste stalk, corn-stalk cellulose (CSC) was extracted by acid–base method and used as modifier of epoxy resin (E51) to prepare the self-extracted corn-stalk cellulose/epoxy resin composites (CSCEC). Differential scanning calorimeter (DSC), thermogravimetry (TG) analysis, dynamic mechanical analysis (DMA), morphology analysis by scanning electron microscope (SEM), the mechanical properties by electronic universal testing machine and impact testing machine were used for characterization and analysis. The experimental results showed that when the CSC content was 20 wt%, the impact strength of the composite was 2.50 kJ/m(2), which was 127.2% higher than that of pure epoxy resin. When the CSC content was 20 wt%, the Tg of epoxy resin obtained by DMA was the lowest, 167.4 °C, which decreased by 11.3 °C compared with that of pure epoxy resin. The SEM result showed that the fracture surface of the composite became obviously rough and had of obvious folds, which was a ductile fracture. These results indicated that the addition of CSC could toughen the epoxy resin. Nature Publishing Group UK 2022-12-05 /pmc/articles/PMC9722901/ /pubmed/36471157 http://dx.doi.org/10.1038/s41598-022-25695-0 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) . |
spellingShingle | Article Lou, Chunhua Jiang, Siyu Yan, An Zhou, Yongli Liu, Yang Zhang, Yong Kong, Xianzhi Self-extracted corn-stalk cellulose/epoxy resin composites |
title | Self-extracted corn-stalk cellulose/epoxy resin composites |
title_full | Self-extracted corn-stalk cellulose/epoxy resin composites |
title_fullStr | Self-extracted corn-stalk cellulose/epoxy resin composites |
title_full_unstemmed | Self-extracted corn-stalk cellulose/epoxy resin composites |
title_short | Self-extracted corn-stalk cellulose/epoxy resin composites |
title_sort | self-extracted corn-stalk cellulose/epoxy resin composites |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9722901/ https://www.ncbi.nlm.nih.gov/pubmed/36471157 http://dx.doi.org/10.1038/s41598-022-25695-0 |
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