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Controlled Morphological Bending of 3D-FEBID Structures via Electron Beam Curing

Focused electron beam induced deposition (FEBID) is one of the few additive, direct-write manufacturing techniques capable of depositing complex 3D nanostructures. In this work, we explore post-growth electron beam curing (EBC) of such platinum-based FEBID deposits, where free-standing, sheet-like e...

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Autores principales: Weitzer, Anna, Winkler, Robert, Kuhness, David, Kothleitner, Gerald, Plank, Harald
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9737864/
https://www.ncbi.nlm.nih.gov/pubmed/36500873
http://dx.doi.org/10.3390/nano12234246
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author Weitzer, Anna
Winkler, Robert
Kuhness, David
Kothleitner, Gerald
Plank, Harald
author_facet Weitzer, Anna
Winkler, Robert
Kuhness, David
Kothleitner, Gerald
Plank, Harald
author_sort Weitzer, Anna
collection PubMed
description Focused electron beam induced deposition (FEBID) is one of the few additive, direct-write manufacturing techniques capable of depositing complex 3D nanostructures. In this work, we explore post-growth electron beam curing (EBC) of such platinum-based FEBID deposits, where free-standing, sheet-like elements were deformed in a targeted manner by local irradiation without precursor gas present. This process diminishes the volumes of exposed regions and alters nano-grain sizes, which was comprehensively characterized by SEM, TEM and AFM and complemented by Monte Carlo simulations. For obtaining controlled and reproducible conditions for smooth, stable morphological bending, a wide range of parameters were varied, which will here be presented as a first step towards using local EBC as a tool to realize even more complex nano-architectures, beyond current 3D-FEBID capabilities, such as overhanging structures. We thereby open up a new prospect for future applications in research and development that could even be further developed towards functional imprinting.
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spelling pubmed-97378642022-12-11 Controlled Morphological Bending of 3D-FEBID Structures via Electron Beam Curing Weitzer, Anna Winkler, Robert Kuhness, David Kothleitner, Gerald Plank, Harald Nanomaterials (Basel) Article Focused electron beam induced deposition (FEBID) is one of the few additive, direct-write manufacturing techniques capable of depositing complex 3D nanostructures. In this work, we explore post-growth electron beam curing (EBC) of such platinum-based FEBID deposits, where free-standing, sheet-like elements were deformed in a targeted manner by local irradiation without precursor gas present. This process diminishes the volumes of exposed regions and alters nano-grain sizes, which was comprehensively characterized by SEM, TEM and AFM and complemented by Monte Carlo simulations. For obtaining controlled and reproducible conditions for smooth, stable morphological bending, a wide range of parameters were varied, which will here be presented as a first step towards using local EBC as a tool to realize even more complex nano-architectures, beyond current 3D-FEBID capabilities, such as overhanging structures. We thereby open up a new prospect for future applications in research and development that could even be further developed towards functional imprinting. MDPI 2022-11-29 /pmc/articles/PMC9737864/ /pubmed/36500873 http://dx.doi.org/10.3390/nano12234246 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Weitzer, Anna
Winkler, Robert
Kuhness, David
Kothleitner, Gerald
Plank, Harald
Controlled Morphological Bending of 3D-FEBID Structures via Electron Beam Curing
title Controlled Morphological Bending of 3D-FEBID Structures via Electron Beam Curing
title_full Controlled Morphological Bending of 3D-FEBID Structures via Electron Beam Curing
title_fullStr Controlled Morphological Bending of 3D-FEBID Structures via Electron Beam Curing
title_full_unstemmed Controlled Morphological Bending of 3D-FEBID Structures via Electron Beam Curing
title_short Controlled Morphological Bending of 3D-FEBID Structures via Electron Beam Curing
title_sort controlled morphological bending of 3d-febid structures via electron beam curing
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9737864/
https://www.ncbi.nlm.nih.gov/pubmed/36500873
http://dx.doi.org/10.3390/nano12234246
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